除虫菊提取物高效液相色谱法的方法开发与验证
Method development and validation of a high-performance liquid chromatographic method for pyrethrum extract.
作者信息
Essig K, Zhao Z
机构信息
Aventis Environmental Science, Montvale, NJ 07645, USA.
出版信息
J Chromatogr Sci. 2001 Nov;39(11):473-80. doi: 10.1093/chromsci/39.11.473.
PMID:11718308
Abstract
A robust analytical methodology is developed for the quantitative determination of all six insecticidal components of pyrethrum extract: jasmolin I, cinerin I, pyrethrin I, jasmolin II, cinerin II, and pyrethrin II. This method, based on the separation technique normal-phase high-performance liquid chromatography, offers selectivity, accuracy, precision, linearity, range, ruggedness, and robustness as well as efficiency and ease.
摘要
开发了一种强大的分析方法，用于定量测定除虫菊提取物的所有六种杀虫成分：茉莉酮菊酯I、瓜叶菊酯I、除虫菊酯I、茉莉酮菊酯II、瓜叶菊酯II和除虫菊酯II。该方法基于正相高效液相色谱分离技术，具有选择性、准确性、精密度、线性、范围、耐用性和稳健性，以及高效性和简便性。
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