Baba N, Taira Y, Matsumura H, Atsuta M
Department of Fixed Prosthodontics, Nagasaki University School of Dentistry, Nagasaki, Japan.
J Oral Rehabil. 2002 May;29(5):478-83. doi: 10.1046/j.1365-2842.2002.00848.x.
The purpose of this study was to evaluate the effects of disinfectants on the bond strength of resin to dentine. The surface of bovine dentine was exposed to formaldehyde (FA) aqueous solutions, glutaraldehyde (GA) aqueous solutions, 2-hydroxyethyl methacrylate aqueous solutions (HEMA), a commercially available dentine primer (Gluma CPS desensitizer, GLUMA), isotonic sodium chloride solution (IS), and distilled water (DW), and placed in a humidor (HU) at 37 degrees C, or non-stored (baseline). All dentine surfaces were conditioned with a 10% citric acid and 3% ferric chloride solution (10-3 liquid), and then bonded to an acrylic rod with a self-curing adhesive resin (Super-Bond C&B). The mean tensile bond strengths determined 24 h after bonding were compared by analysis of variance (ANOVA) and Fisher's protected LSD test (n=5, P < or = 0.05). The exposure of dentine to IS, DW and HU for both 48 and 168 h resulted in a decrease in bond strength when compared with the baseline. The highest bond strengths after 168 h of exposure were obtained with 5% GA, 10% HEMA, and GLUMA, the values of which were equivalent to baseline and were significantly higher than that of FA. It is concluded that disinfectant pre-treatment with 5% GA or GLUMA stabilizes the bonding of tri-n-butylborane (TBB) initiated luting agent to bovine dentine conditioned with 10-3 liquid.
本研究的目的是评估消毒剂对树脂与牙本质粘结强度的影响。将牛牙本质表面暴露于甲醛(FA)水溶液、戊二醛(GA)水溶液、甲基丙烯酸羟乙酯水溶液(HEMA)、一种市售牙本质底漆(Gluma CPS脱敏剂,GLUMA)、等渗氯化钠溶液(IS)和蒸馏水中,然后置于37℃的保湿箱(HU)中,或不进行储存(基线)。所有牙本质表面均用10%柠檬酸和3%氯化铁溶液(10 - 3液)进行预处理,然后用自固化粘结树脂(Super - Bond C&B)粘结到丙烯酸棒上。通过方差分析(ANOVA)和Fisher保护最小显著差异检验比较粘结24小时后测定的平均拉伸粘结强度(n = 5,P≤0.05)。与基线相比,牙本质暴露于IS、DW和HU 48小时和168小时后粘结强度均降低。暴露168小时后,5% GA、10% HEMA和GLUMA获得的粘结强度最高,其值与基线相当,且显著高于FA。得出的结论是,用5% GA或GLUMA进行消毒剂预处理可稳定三正丁基硼烷(TBB)引发的粘结剂与经10 - 3液预处理的牛牙本质的粘结。