Yamasaki Jun, Kawai Tomoyuki, Tanaka Nobuo
EcoTopia Science Institute and Department of Crystalline Materials Science, Nagoya University, Chikusa-ku, Nagoya, 464-8603, Japan.
J Electron Microsc (Tokyo). 2005 Jun;54(3):209-14. doi: 10.1093/jmicro/dfi029. Epub 2005 Aug 25.
A simple and practical method for minimizing non-linear image contrast in spherical aberration-corrected (C(S)-corrected) high-resolution transmission electron microscopy is presented. The effectiveness of the method is considered from the viewpoints of theoretical formulations and image simulations including second-order imaging effects. The method is one of the advantages of C(S)-correction and applied to high-resolution images down to 0.1 nm. The dynamical diffraction effect is carefully evaluated, which shows that the phase deviation of diffracted waves from pi/2 violates the present method in thicker crystals over approximately 10 nm.
提出了一种在球差校正(C(S)校正)高分辨率透射电子显微镜中最小化非线性图像对比度的简单实用方法。从理论公式和包括二阶成像效应的图像模拟的角度考虑了该方法的有效性。该方法是C(S)校正的优点之一,并应用于低至0.1 nm的高分辨率图像。仔细评估了动态衍射效应,结果表明,在厚度超过约10 nm的较厚晶体中,衍射波相对于π/2的相位偏差会使本方法失效。