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固化设备和染色溶液对树脂复合材料颜色稳定性的影响。

The effect of curing units and staining solutions on the color stability of resin composites.

作者信息

Yazici A Rüya, Celik Cigdem, Dayangaç Berrin, Ozgünaltay Gül

机构信息

Hacettepe University, Faculty of Dentistry, Department of Conservative Dentistry, Ankara, Turkey.

出版信息

Oper Dent. 2007 Nov-Dec;32(6):616-22. doi: 10.2341/07-3.

Abstract

This study investigated the effects of two different light curing units and two staining solutions on the color stability of a hybrid composite and a nanohybrid composite after different immersion periods. Thirty disk-shaped specimens (10 mm in diameter, 2-mm thick) were fabricated for each of the resin composites, Clearfil AP-X and Filtek Supreme. The specimens were randomly divided into two groups according to the curing unit used: Group I specimens (n = 15) were cured with a quartz-tungsten-halogen (QTH) light for 40 seconds, and Group II specimens (n = 15) were cured with a light-emitting diode (LED) unit in standard mode for 40 seconds. The specimens were incubated in 100% humidity at 37 degrees C for 24 hours. Then, the baseline color values (L*, a*, b*) of each specimen were measured with a spectrophotometer according to the CIELab color scale. After baseline color measurements, five randomly selected specimens from each group (Groups I and II) were immersed in one of two staining solutions (tea or coffee) or distilled water (control). After 1, 7 and 30 days of immersion, the color values of each specimen were remeasured and the color change value (deltaE*ab) calculated. Color changes caused by immersion in tea and coffee for 30 days were only perceptible in the Clearfil AP-X specimens cured with QTH or LED. In the Filtek Supreme specimens, coffee perceptibly stained the teeth after all immersion periods and tea stained after 30 days. Polymerization with QTH or LED did not cause any significant difference in the color stability of Clearfil AP-X or Filtek Supreme. While there were no significant differences between staining solutions in the Clearfil AP-X specimens cured with LED after one and seven days of storage and one day of storage in the QTH cured specimens, significant differences were observed between water and coffee after seven days of storage. In the Filtek Supreme specimens cured with QTH or LED, there were statistically significant differences between the staining solutions after one and seven days of storage. After 30 days of storage, no significant difference was found between tea and coffee in either resin composite cured with QTH or LED. The effect of the staining solutions (tea, coffee) on color changes in composites was immersion time and resin-material dependent.

摘要

本研究调查了两种不同的光固化机和两种染色溶液对混合复合树脂和纳米混合复合树脂在不同浸泡时间后的颜色稳定性的影响。为每种树脂复合材料(Clearfil AP-X和Filtek Supreme)制作了30个圆盘形试件(直径10毫米,厚2毫米)。根据所使用的固化机,将试件随机分为两组:第一组试件(n = 15)用石英卤钨灯(QTH)光固化40秒,第二组试件(n = 15)用发光二极管(LED)光固化机在标准模式下固化40秒。将试件在37℃、湿度100%的条件下孵育24小时。然后,根据CIELab色标用分光光度计测量每个试件的基线颜色值(L*、a*、b*)。在进行基线颜色测量后,从每组(第一组和第二组)中随机选取五个试件,将其浸入两种染色溶液(茶或咖啡)之一或蒸馏水中(对照)。在浸泡1、7和30天后,重新测量每个试件的颜色值并计算颜色变化值(ΔE*ab)。仅在用QTH或LED固化的Clearfil AP-X试件中,能察觉到浸泡在茶和咖啡中30天引起的颜色变化。在Filtek Supreme试件中,在所有浸泡时间后咖啡均能明显使牙齿染色,茶在30天后染色。用QTH或LED固化对Clearfil AP-X或Filtek Supreme的颜色稳定性没有造成任何显著差异。在用LED固化的Clearfil AP-X试件储存1天和7天后以及用QTH固化的试件储存1天后,染色溶液之间没有显著差异,但在储存7天后观察到水和咖啡之间存在显著差异。在用QTH或LED固化的Filtek Supreme试件中,储存1天和7天后染色溶液之间存在统计学上的显著差异。在储存30天后,在用QTH或LED固化的两种树脂复合材料中,茶和咖啡之间均未发现显著差异。染色溶液(茶、咖啡)对复合材料颜色变化的影响取决于浸泡时间和树脂材料。

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