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用于广泛高压测量的微型金刚石对顶砧室。

Miniature diamond anvil cell for broad range of high pressure measurements.

作者信息

Gavriliuk A G, Mironovich A A, Struzhkin V V

机构信息

Geophysical Laboratory, Carnegie Institution of Washington, 5251 Broad Branch Road NW, Washington, DC 20015, USA.

出版信息

Rev Sci Instrum. 2009 Apr;80(4):043906. doi: 10.1063/1.3122051.

Abstract

A miniature versatile nonmagnetic diamond anvil cell for diverse physical property measurement under cryogenic environments and high magnetic fields at high pressure has been developed. Several such cells have been manufactured and tested in the Physical Properties Measurement System (PPMS) by Quantum Design at high pressures and low temperatures. The cells have good pressure stability during temperature scans down to helium temperatures and back to room temperature. The cells have been tested in strong magnetic fields and demonstrated excellent nonmagnetic properties. The wide-angle side openings give the possibility to use this cell as a "panoramic cell" in synchrotron experiments requiring large angle off-axis access. The possible experiments, which may use this cell, include spectroscopic experiments (optical, synchrotron Mossbauer, Raman, x-ray emission, etc.), different types of x-ray diffraction experiments, transport measurements (resistivity, magnetoresistivity, thermoelectromotive force, etc.), measurements of susceptibility, and many other conventional and synchrotron experiments at very low temperatures and in strong magnetic fields.

摘要

已开发出一种微型多功能非磁性金刚石对顶砧盒,用于在低温环境、高压和强磁场下进行多种物理性质测量。已制造了几个这样的盒子,并在Quantum Design公司的物理性质测量系统(PPMS)中进行了高压和低温测试。这些盒子在温度扫描至氦温度并回到室温的过程中具有良好的压力稳定性。这些盒子已在强磁场中进行了测试,并表现出优异的非磁性特性。广角侧面开口使该盒子有可能在需要大角度离轴访问的同步加速器实验中用作“全景盒”。可能使用该盒子的实验包括光谱实验(光学、同步加速器穆斯堡尔、拉曼、x射线发射等)、不同类型的x射线衍射实验、输运测量(电阻率、磁电阻率、热电动势等)、磁化率测量,以及许多其他在极低温和强磁场下的传统实验和同步加速器实验。

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