Morks M F, Kobayashi A
Central Metallurgical Research and Development Institute, PO Box 87, Helwan, El-tibben, Cairo, Egypt.
J Mech Behav Biomed Mater. 2008 Apr;1(2):165-71. doi: 10.1016/j.jmbbm.2007.09.002. Epub 2007 Oct 5.
Gas tunnel-type plasma spraying (GTPS) was employed to deposit ZrO(2)/SiO(2) bioinert ceramic composite coatings with an appropriate thickness on SUS 304 substrate. Zirconia and fused silica powders, with equal wt%, have been mixed together in ceramic pot for 30 min and internally fed in the plasma jet. The composite coatings were sprayed at two different gas flow rates (120 and 150 l/min) and constant vortex arc current of 450 A and gun current of 50 A. The microstructure of as-sprayed coatings was examined by scanning electron microscope. Elemental analysis was achieved for the composite coatings using EDS analysis unit which is attached to SEM. Phase structure was investigated by X-ray diffraction. The hardness and abrasive wear test of the coatings were investigated. The biological property of the coatings was examined by immersing the as-sprayed coatings in simulated body fluid (SBF) solution for 20 days at 36.5 degrees C. The growth of apatite (HA) on the coatings surfaces was observed by SEM and EDX analysis.
采用气体隧道式等离子喷涂(GTPS)在SUS 304基体上制备了具有适当厚度的ZrO(2)/SiO(2)生物惰性陶瓷复合涂层。将等重量百分比的氧化锆和熔融石英粉末在陶瓷罐中混合30分钟,然后送入等离子射流内部。复合涂层在两种不同的气体流量(120和150升/分钟)以及450 A的恒定涡旋电弧电流和50 A的喷枪电流下进行喷涂。通过扫描电子显微镜检查喷涂态涂层的微观结构。使用附着在扫描电子显微镜上的能谱分析单元对复合涂层进行元素分析。通过X射线衍射研究相结构。研究了涂层的硬度和耐磨性能。通过将喷涂态涂层在36.5℃的模拟体液(SBF)溶液中浸泡20天来检查涂层的生物学性能。通过扫描电子显微镜和能谱分析观察涂层表面磷灰石(HA)的生长情况。