Golubeva A V, Mayer M, Gasparyan Yu M, Roth J, Kurnaev V A
RRC Kurchatov Institute, Ac. Kurchatov sq., 1/1, Moscow RU-123182, Russia.
Rev Sci Instrum. 2009 Jul;80(7):073501. doi: 10.1063/1.3154385.
A new installation PERMEX for the investigation of ion-driven permeation through metals was designed and built. A metal membrane under investigation separates two high-vacuum chambers. In the implantation chamber, the membrane surface is irradiated with a monoenergetic deuterium ion beam with an incident energy in the interval of 100-3000 eV/D. The ion flux at the surface is in a range of 10(13)-2 x 10(14) D/cm2 s, the membrane temperature can be varied in the interval of 290-1050 K. The permeating deuterium flux from the outlet membrane surface to the volume of the second chamber (registration chamber) is measured by a quadrupole mass-analyzer. The outlet surface of the membrane can be cleaned by an argon ion beam. To approve the correct work of the setup a number of experiments were performed with Ni membranes. First results of experiments with tungsten membranes are presented.
设计并制造了一种用于研究离子驱动通过金属渗透的新装置PERMEX。一个正在研究的金属膜将两个高真空腔室隔开。在注入腔室中,用能量在100 - 3000 eV/D区间的单能氘离子束照射膜表面。表面的离子通量在10(13)-2×10(14) D/cm2 s范围内,膜温度可在290 - 1050 K区间内变化。从膜出口表面到第二腔室(记录腔室)体积的渗透氘通量由四极质量分析仪测量。膜的出口表面可用氩离子束清洁。为验证该装置的正常工作,用镍膜进行了一系列实验。给出了钨膜实验的初步结果。