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N'-(5-Bromo-2-hydr-oxy-3-methoxy-benzyl-idene)isonicotinohydrazide.

作者信息

Peng San-Jun, Hou Hai-Yun

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Sep 24;64(Pt 10):o1995. doi: 10.1107/S1600536808029607.

Abstract

The title compound, C(14)H(12)BrN(3)O(3), was prepared by reaction of 5-bromo-3-methoxy-salicylaldehyde and isonicotinohydrazide in methanol. The mol-ecule is not planar and adopts a trans configuration with respect to the C=N bond. There is an intra-molecular O-H⋯N hydrogen bond in the mol-ecule. The dihedral angle between the benzene and pyridine rings is 12.2 (2)°. In the crystal structure, mol-ecules are linked through inter-molecular N-H⋯N hydrogen bonds, forming chains running along the c-axis direction.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/366f/2959402/28ffcb01d7f7/e-64-o1995-fig1.jpg

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