Tercan Barış, Sahin Ertan, Patır Süleyman, Hökelek Tuncer
Acta Crystallogr Sect E Struct Rep Online. 2010 Jan 9;66(Pt 2):o328. doi: 10.1107/S160053681000067X.
The title compound, C(20)H(24)N(2)O(2)S(2), consists of a tetra-cyclic ring system containing an azocino skeleton with ethyl, dithiol-ane and methoxy-methyl groups as substituents. The benzene and five-membered rings are nearly coplanar, with a dihedral angle of 2.78 (11)°. The dithiol-ane ring adopts an envelope conformation. In the crystal structure, inter-molecular C-H⋯O hydrogen bonds link the mol-ecules into chains nearly parallel to the c axis. Two C-H⋯π inter-actions are also present.
标题化合物C(20)H(24)N(2)O(2)S(2)由一个四环体系组成,该体系包含一个偶氮辛环骨架,带有乙基、二硫戊环和甲氧基甲基作为取代基。苯环和五元环几乎共面,二面角为2.78 (11)°。二硫戊环环采取信封构象。在晶体结构中,分子间的C-H⋯O氢键将分子连接成几乎平行于c轴的链。还存在两种C-H⋯π相互作用。