Department of Mechanical Engineering, University of British Columbia, Vancouver, BC, Canada.
J Mater Sci Mater Med. 2012 Feb;23(2):349-56. doi: 10.1007/s10856-011-4513-2. Epub 2011 Dec 20.
This paper reports electrochemical polishing (EP) of 316L stainless-steel structures patterned using micro-electro-discharge machining (μEDM) for application to stents including intelligent stents based on micro-electro-mechanical-systems technologies. For the process optimization, 10 μm deep cavities μEDMed on the planar material were polished in a phosphoric acid-based electrolyte with varying current densities and polishing times. The EP condition with a current density of 1.5 A/cm(2) for an EP time of 180 s exhibited the highest surface quality with an average roughness of 28 nm improved from~400 nm produced with high-energy μEDM. The EP of μEDMed surfaces was observed to produce almost constant smoothness regardless of the initial roughness determined by varying discharge energies. Energy-dispersive X-ray spectroscopy was performed on the μEDMed surfaces before and after EP. A custom rotational apparatus was used to polish tubular test samples including stent-like structures created using μEDM, demonstrating uniform removal of surface roughness and sharp edges from the structures.
本文报告了电化学抛光(EP)技术在微电放电加工(μEDM)图案化的 316L 不锈钢结构中的应用,该技术可应用于支架,包括基于微机电系统技术的智能支架。为了进行工艺优化,在磷酸基电解液中对平面材料上深达 10 μm 的腔体进行了抛光,电流密度和抛光时间有所不同。在电流密度为 1.5 A/cm(2)、EP 时间为 180 s 的 EP 条件下,表面质量最高,平均粗糙度从高能 μEDM 产生的约 400 nm 提高到 28 nm。观察到 EP 对 μEDMed 表面的作用几乎使粗糙度保持恒定,而初始粗糙度由放电能量的不同决定。在 EP 前后对 μEDMed 表面进行了能量色散 X 射线光谱分析。使用定制的旋转装置对管状测试样品进行了抛光,包括使用 μEDM 制造的支架状结构,从结构上均匀去除了表面粗糙度和锐边。