Department of Dental Materials and Prosthodontics, São Paulo State University-UNESP, São Paulo, Brazil.
Clin Oral Investig. 2013 Jan;17(1):325-31. doi: 10.1007/s00784-011-0668-y. Epub 2012 Jan 13.
The aim of this study was to evaluate the effect of different seating forces during cementation in cement-ceramic microtensile bond strength (μTBS).
Forty-five blocks (5 × 5 × 4 mm(3)) of a glass-infiltrated alumina-based ceramic (In-Ceram Alumina) were fabricated according to the manufacturer's instructions and duplicated in resin composite. Ceramic surfaces were polished, cleaned for 10 min in an ultrasonic bath, silica coated using a laboratory type of air abrasion device, and silanized. Each treated ceramic block was then randomly assigned to five groups (n = 9) and cemented to a composite block under five seating forces (10 g, 50 g, 100 g, 500 g, and 750 g) using a dual-cured resin cement (Panavia F). The ceramic-cement-composite assemblies were cut under coolant water to obtain bar specimens (1 mm × 0.8 mm(2)). The μTBS tests were performed in a universal testing machine (1 mm/min). The mean bond strengths values were statistically analyzed using one-way ANOVA (α ≤ 0.05).
Different seating forces resulted in no significant difference in the μTBS results ranging between 13.1 ± 4.7 and 18.8 ± 2.1 MPa (p = 0.13) and no significant differences among cement thickness.
Excessive seating forces during cementation seem not to affect the μTBS results.
Excessive forces during the seating of single all-ceramic restorations cementation seem to display the same tensile bond strength to the resin cement.
本研究旨在评估不同粘结剂加压对陶瓷-树脂微拉伸粘结强度(μTBS)的影响。
根据制造商的说明制作 45 个玻璃渗透氧化铝基陶瓷(In-Ceram Alumina)块(5×5×4mm³),并在树脂复合材料中复制。陶瓷表面经过抛光、在超声浴中清洗 10 分钟、使用实验室型空气喷砂装置涂覆二氧化硅并硅烷化。每个处理过的陶瓷块随后随机分配到五个组(n=9),并在五种不同的坐压力(10g、50g、100g、500g 和 750g)下使用双固化树脂粘结剂(Panavia F)粘结到复合块上。在冷却剂下切割陶瓷-粘结剂-复合材料组件,以获得条状样本(1mm×0.8mm²)。在万能试验机上以 1mm/min 的速度进行 μTBS 测试。使用单因素方差分析(α≤0.05)对平均粘结强度值进行统计学分析。
不同的坐压力导致 μTBS 结果在 13.1±4.7 和 18.8±2.1MPa 之间没有显著差异(p=0.13),粘结剂厚度之间也没有显著差异。
在粘结过程中施加过大的坐压力似乎不会影响 μTBS 结果。
在单全瓷修复体粘结时施加过大的坐压力似乎不会对树脂粘结剂的拉伸粘结强度产生影响。