State Key Laboratory for Mesoscopic Physics, and Electron Microscopy Laboratory, School of Physics, Peking University, Beijing, People's Republic of China.
Nanotechnology. 2012 Mar 2;23(8):085301. doi: 10.1088/0957-4484/23/8/085301. Epub 2012 Feb 1.
A poly(methyl methacrylate) assisted dry transfer method was developed to transfer graphene microflake onto a suspended SiN chip in an effective and efficient way for further graphene nanopore drilling for DNA analysis. Graphene microflakes can be patterned by e-beam lithography to a designed shape and size on a large scale of a few thousands simultaneously. Subsequently, individual graphene microflakes can be picked up and transferred to a target hole on a suspended SiN membrane with 1 µm precision via a site-specific transfer-printing method. Nanopores with different diameters from 3 to 20 nm were drilled on the as-transferred graphene membrane in a transmission electron microscope. This method offers a fast and controllable way to fabricate graphene nanopores for DNA analyses.
一种聚甲基丙烯酸甲酯(PMMA)辅助干法转移方法被开发出来,以有效地将石墨烯微片转移到悬浮的氮化硅(SiN)芯片上,以便进一步在石墨烯纳米孔中进行 DNA 分析。石墨烯微片可以通过电子束光刻在几万个同时进行的大面积上图案化为设计的形状和尺寸。随后,通过特定位置的转印打印方法,单个石墨烯微片可以被拾取并转移到悬浮的 SiN 膜上的目标孔中,精度达到 1 µm。在传输电子显微镜中,在转移的石墨烯膜上钻取了直径从 3 到 20nm 的不同直径的纳米孔。该方法为 DNA 分析提供了一种快速可控的制造石墨烯纳米孔的方法。