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N'-(3-Fluoro-benzyl-idene)-4-hy-droxy-3-meth-oxy-benzohydrazide methanol monosolvate.

作者信息

Zong Qian-Shou

机构信息

College of Biology and Chemical Engineering, Jiaxing University, Jiaxing Zhejiang 314001, People's Republic of China, and School of Pharmaceutical Sciences, Zhejiang University, Hangzhou Zhejiang 310058, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 May 1;68(Pt 5):o1338. doi: 10.1107/S1600536812012196. Epub 2012 Apr 6.

Abstract

In the title compound, C(15)H(13)FN(2)O(3)·CH(3)OH, the dihedral angle between the benzene rings of the benzohydrazone mol-ecule is 5.3 (3)°. The C atom of the meth-oxy group is almost coplanar with its attached ring [deviation = 0.017 (2) Å]. The r.m.s. deviation of the 21 non-H atoms of the hydrazone mol-ecule is 0.106 Å. In the crystal, the components are linked by O(m)-H⋯O(h), N(h)-H⋯O(m) and O(h)-H⋯O(h) (m = methanol and h = hydrazone) hydrogen bonds, forming (001) layers.

摘要

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