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基于吸收微波能的微波辅助提取提取曲线的建模与预测。

Modeling and prediction of extraction profile for microwave-assisted extraction based on absorbed microwave energy.

机构信息

University of Malaya, Department of Chemical Engineering, 50603 Kuala Lumpur, Malaysia.

出版信息

Food Chem. 2013 Sep 1;140(1-2):147-53. doi: 10.1016/j.foodchem.2013.02.057. Epub 2013 Feb 24.

Abstract

A modeling technique based on absorbed microwave energy was proposed to model microwave-assisted extraction (MAE) of antioxidant compounds from cocoa (Theobroma cacao L.) leaves. By adapting suitable extraction model at the basis of microwave energy absorbed during extraction, the model can be developed to predict extraction profile of MAE at various microwave irradiation power (100-600 W) and solvent loading (100-300 ml). Verification with experimental data confirmed that the prediction was accurate in capturing the extraction profile of MAE (R-square value greater than 0.87). Besides, the predicted yields from the model showed good agreement with the experimental results with less than 10% deviation observed. Furthermore, suitable extraction times to ensure high extraction yield at various MAE conditions can be estimated based on absorbed microwave energy. The estimation is feasible as more than 85% of active compounds can be extracted when compared with the conventional extraction technique.

摘要

提出了一种基于吸收微波能量的建模技术,用于模拟从可可(Theobroma cacao L.)叶中提取抗氧化化合物的微波辅助提取(MAE)。通过在提取过程中吸收的微波能量的基础上适应合适的提取模型,可以开发该模型来预测在各种微波辐射功率(100-600 W)和溶剂装载量(100-300 ml)下的 MAE 提取曲线。通过与实验数据进行验证,证实该预测能够准确捕捉 MAE 的提取曲线(R 方值大于 0.87)。此外,模型预测的产率与实验结果吻合良好,观察到的偏差小于 10%。此外,还可以根据吸收的微波能量来估计在各种 MAE 条件下确保高提取产率所需的合适提取时间。这种估计是可行的,因为与传统提取技术相比,当提取 85%以上的活性化合物时,就能达到较高的提取率。

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