Department of Physics, Annamalai University, Annamalainagar 608 002, Tamil Nadu, India.
Spectrochim Acta A Mol Biomol Spectrosc. 2013 Nov;115:388-92. doi: 10.1016/j.saa.2013.06.050. Epub 2013 Jun 28.
The present work focuses the use of aqueous extract of Gloriosa superba Linn. (Glory Lily) for producing silver nanoparticles (AgNPs) from silver nitrate aqueous solution. Phytochemical analysis of the extract revealed the presence of alkaloid, amino acids, carbohydrates and proteins in the extract and they serve as effective reducing and capping agents for converting silver nitrate to silver nanoparticles. The nanoparticles were characterised by UV (Ultra violet), FT-IR (Fourier Transform Infrared), XRD (X-ray diffraction), TEM (Transmission Electron Microscope) SEM-EDX (Scanning Electron Microscopy-Energy Dispersive X-ray), and PL (Photoluminescence) studies. Moreover, the catalytic activity of synthesized AgNPs in the reduction of methylene blue was studied by UV-vis spectrophotometer. The synthesized AgNPs are observed to have a good catalytic activity on the reduction of methylene blue by G. superba extract which is confirmed by the decrease in absorbance maximum values of methylene blue with respect to time using UV-vis spectrophotometer.
本研究聚焦于利用百子莲(Gloriosa superba Linn.)的水提物从硝酸银水溶液中制备银纳米粒子(AgNPs)。提取物的植物化学分析表明,提取物中存在生物碱、氨基酸、碳水化合物和蛋白质,它们可作为有效的还原剂和稳定剂,将硝酸银转化为银纳米粒子。通过紫外(UV)、傅里叶变换红外(FT-IR)、X 射线衍射(XRD)、透射电子显微镜(TEM)、扫描电子显微镜-能谱(SEM-EDX)和光致发光(PL)研究对纳米粒子进行了表征。此外,还通过紫外-可见分光光度计研究了合成的 AgNPs 在还原亚甲基蓝中的催化活性。通过紫外-可见分光光度计观察到,用百子莲提取物还原亚甲基蓝时,合成的 AgNPs 具有良好的催化活性,这可以通过亚甲基蓝的最大吸收值随时间的降低来证实。