室温下使用五氧化二磷-甲磺酸混合物快速绿色一锅法合成3,4-二氢嘧啶-2(1H)-酮
A Green, Expeditious, One-Pot Synthesis of 3, 4-Dihydropyrimidin-2(1H)-ones Using a Mixture of Phosphorus Pentoxide-Methanesulfonic Acid at Ambient Temperature.
作者信息
Borse Amulrao, Patil Mahesh, Patil Nilesh, Shinde Rohan
机构信息
School of Chemical Sciences, North Maharashtra University, Jalgaon 425 001, India.
出版信息
ISRN Org Chem. 2012 Aug 8;2012:415645. doi: 10.5402/2012/415645. eCollection 2012.
Abstract
An expeditious, one-pot method for the synthesis of 3,4-dihydropyrimidin-2(1H)-ones using a mixture of phosphorus pentoxide-methanesulfonic acid (Eaton's reagent) at room temperature under solvent-free conditions is described. The salient features of this method include short reaction time, green aspects, high yields, and simple procedure.
摘要
描述了一种在无溶剂条件下于室温使用五氧化二磷 - 甲磺酸混合物（伊顿试剂）快速一锅法合成3,4 - 二氢嘧啶 - 2(1H)-酮的方法。该方法的显著特点包括反应时间短、绿色环保、产率高以及操作步骤简单。
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