Siddiqui M Z, Thomas M, Prasad N
Processing and Product Development Division, Indian Institute of Natural Resins & Gums, Namkum, Ranchi-834 010, India.
Indian J Pharm Sci. 2013 May;75(3):368-72. doi: 10.4103/0250-474X.117422.
The present study reports physicochemical characterization and antioxidant activity of essential oils extracted from guggul (Commiphora wightii) exudates collected from different places in Madhya Pradesh, India. The guggul exudates were hydrodistilled for 3-4 h in Clevenger apparatus. The oil obtained was dried over anhydrous Na2SO4 and stored at 4° until testing. Before extraction of oils from the exudates, their % moisture and tristimulus values of the colors namely L (white-black), a (green-red) and b (blue-yellow) were determined. Physicochemical characterization of the extracted oils was carried out to determine their solubility, yield%, acid value (mg/KOH/g), saponification value (mg/KOH/g), ester value, iodine value (g/g), peroxide value (mEq/kg) and Fourier transformed infrared analyses. The storage-effect on the % moisture and tristimulus values of the colors of guggul exudates as also the % oil yield and physicochemical parameters of the essential oils extracted from them, were studied using three different packaging materials viz., local plastic, low density polyethylene (200 G) and high density polyethylene (200 G). The antioxidant potential of extracted oils was evaluated by free radical scavenging activity using 1,1-diphenyl-2-picryl hydrazyl assay.
本研究报告了从印度中央邦不同地点采集的古古勒(Commiphora wightii)渗出物中提取的精油的物理化学特性和抗氧化活性。古古勒渗出物在克利夫兰装置中进行水蒸馏3 - 4小时。所得的油用无水硫酸钠干燥,并在4°C下储存直至测试。在从渗出物中提取油之前,测定了它们的水分百分比以及颜色的三刺激值,即L(白 - 黑)、a(绿 - 红)和b(蓝 - 黄)。对提取的油进行物理化学特性分析,以确定其溶解度、产率%、酸值(mg/KOH/g)、皂化值(mg/KOH/g)、酯值、碘值(g/g)、过氧化值(mEq/kg)以及傅里叶变换红外分析。使用三种不同的包装材料,即当地塑料、低密度聚乙烯(200 G)和高密度聚乙烯(200 G),研究了储存对古古勒渗出物的水分百分比和颜色三刺激值以及从中提取的精油的油产率%和物理化学参数的影响。通过使用1,1 - 二苯基 - 2 - 苦基肼基测定法的自由基清除活性评估提取油的抗氧化潜力。