Chemistry Department, Faculty of Science, Menoufia University, Egypt.
Spectroscopy Department, Physics Division, National Research Center (NRC), Egypt.
Spectrochim Acta A Mol Biomol Spectrosc. 2014;121:238-44. doi: 10.1016/j.saa.2013.10.092. Epub 2013 Nov 1.
A green synthesis route was reported to explore the reducing and capping potential of Phoenix dactylifera extract for the synthesis of gold nanoparticles. The processes of nucleation and growth of gold nanoparticles were followed by monitoring the absorption spectra during the reaction. The size and morphology of these nanoparticles was typically imaged using transmission electron microscopy (TEM). The particle size ranged between 32 and 45 nm and are spherical in shape. Fourier transform infrared (FTIR) analysis suggests that the synthesized gold nanoparticles might be stabilized through the interactions of hydroxyl and carbonyl groups in the carbohydrates, flavonoids, tannins and phenolic acids present in P. dactylifera. The as-synthesized Au colloids exhibited good catalytic activity for the degradation of 4-nitrophenol.
报道了一种绿色合成路线,以探索 Phoenix dactylifera 提取物的还原和封端潜力,用于合成金纳米粒子。通过在反应过程中监测吸收光谱来跟踪金纳米粒子的成核和生长过程。使用透射电子显微镜 (TEM) 对这些纳米粒子的尺寸和形态进行典型成像。这些纳米粒子的粒径在 32nm 至 45nm 之间,呈球形。傅里叶变换红外 (FTIR) 分析表明,合成的金纳米粒子可能通过碳水化合物、类黄酮、单宁和存在于 P. dactylifera 中的酚酸中的羟基和羰基之间的相互作用而稳定。所合成的 Au 胶体对 4-硝基苯酚的降解表现出良好的催化活性。