Vaibhav Vineet, Vijayalakshmi U, Roopan S Mohana
Materials Chemistry Division, School of Advanced Sciences, VIT University, Vellore 632 014, India.
Materials Chemistry Division, School of Advanced Sciences, VIT University, Vellore 632 014, India.
Spectrochim Acta A Mol Biomol Spectrosc. 2015 Mar 15;139:515-20. doi: 10.1016/j.saa.2014.12.083. Epub 2014 Dec 27.
The major interest of the paper deals with the extraction of silica from four natural sources such as rice husk, bamboo leaves, sugarcane bagasse and groundnut shell. These waste materials in large quantities can create a serious environmental problem. Hence, there is a need to adopt proper strategy to reduce the waste. In the present investigation, all the waste materials are subjected to moisture removal in a hot plate and sintered at 900°C for 7 h. The sintered powder was treated with 1 M NaOH to form sodium silicate and then with 6M H2SO4 to precipitate silica. The prepared silica powders were characterized by FT-IR, XRD and SEM-EDAX analysis. The silica recovered from different sources was found to vary between 52% and 78%. Magnesium substituted silica was formed from the groundnut waste and further treatment is required to precipitate silica.
该论文的主要兴趣在于从稻壳、竹叶、甘蔗渣和花生壳这四种天然来源中提取二氧化硅。大量的这些废料会造成严重的环境问题。因此,需要采取适当的策略来减少废料。在本研究中,所有废料在热板上进行除湿处理,并在900°C下烧结7小时。将烧结粉末用1M氢氧化钠处理以形成硅酸钠,然后用6M硫酸处理以沉淀二氧化硅。通过傅里叶变换红外光谱(FT-IR)、X射线衍射(XRD)和扫描电子显微镜-能谱分析(SEM-EDAX)对制备的二氧化硅粉末进行表征。发现从不同来源回收的二氧化硅在52%至78%之间变化。从花生废料中形成了镁取代的二氧化硅,需要进一步处理以沉淀二氧化硅。