Gürbüz Serkan, Özmen Monkul Bahar, İpeksaç Tuğba, Gürtekin Seden Merve, Erol Melek
TUBITAK Marmara Research Center, Chemistry Institute, 41470, Gebze, Kocaeli, Turkey.
J Forensic Sci. 2015 May;60(3):727-36. doi: 10.1111/1556-4029.12719. Epub 2015 Feb 17.
This study intends to design magnetite (Fe3 O4 )-based magnetic fingerprint powders with different particle size distributions. It also investigates the influence of particle size distribution on the visualization of latent fingermarks with as little background staining as possible on the surfaces with various porosities in a systematic way. Two strategies were used to prepare the magnetic fingerprint formulations for this study: milling of coarse magnetite particles for different durations, and mixing of sieved fine particles with different size ranges with coarse particles. Particle size analyses of the prepared magnetic powders, optical microscopy-based roughness analysis of the surfaces and SEM measurements of the visualized fingerprints and representative powders were performed. Mag2 of the formulations prepared through milling and Mag5 and Mag6 of the formulations prepared through sieving and mixing were more successful in the development of latent prints than the rest of the solutions.
本研究旨在设计具有不同粒度分布的基于磁铁矿(Fe3O4)的磁性指纹粉。它还系统地研究了粒度分布对在各种孔隙率表面上以尽可能少的背景染色来显现潜在指纹的影响。本研究采用两种策略来制备磁性指纹配方:对粗磁铁矿颗粒进行不同时长的研磨,以及将不同粒径范围的筛分细颗粒与粗颗粒混合。对制备的磁性粉末进行了粒度分析,对表面进行了基于光学显微镜的粗糙度分析,并对显现出的指纹和代表性粉末进行了扫描电子显微镜测量。通过研磨制备的配方中的Mag2以及通过筛分和混合制备的配方中的Mag5和Mag6在潜在指纹显影方面比其他溶液更成功。