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不同实验室及椅旁抛光方案后聚醚醚酮的表面特性

Surface properties of polyetheretherketone after different laboratory and chairside polishing protocols.

作者信息

Heimer Sina, Schmidlin Patrick R, Roos Malgorzata, Stawarczyk Bogna

机构信息

Medical Doctor and Dentist, Department of Prosthodontics, Ludwig-Maximilians-University, Munich, Germany.

Head, Discipline of Periodontology and Peri-Implant Diseases, Clinic of Preventive Dentistry, Periodontology and Cariology, Center of Dental Medicine, University of Zurich, Switzerland.

出版信息

J Prosthet Dent. 2017 Mar;117(3):419-425. doi: 10.1016/j.prosdent.2016.06.016. Epub 2016 Sep 28.

Abstract

STATEMENT OF PROBLEM

Polyetheretherketone (PEEK) can be used as a framework material for fixed dental prostheses. However, information about laboratory and chairside polishing methods is still scarce.

PURPOSE

The purpose of this in vitro study was to determine the effects of laboratory and chairside polishing methods on the surface roughness (SR) and surface free energy (SFE) of PEEK, an autopolymerizing poly(methyl methacrylate), and a veneering composite resin.

MATERIAL AND METHODS

For each of the 3 materials, 80 specimens were prepared (N=240) and divided into 7 polishing groups and 1 control group (n=10). The 7 groups were split into 4 laboratory protocols: polishing paste (Abraso), a second polishing paste (Opal L), silicone polisher (Ceragum), and diamond grinder (Diagen-Turbo grinder). The other 3 groups were chairside protocols: rainbow technique (Super-Snap kit), polishing paste (Prisma gloss), and a polishing system (Enhance finishing). Machine polishing with SiC P4000 served as the control treatment. The protocols' average SRs and SFEs were measured, and their surface topographies were evaluated with scanning electron microscopy (SEM). The logarithmically transformed data were analyzed using covariance analysis, 2-way and 1-way ANOVA, and partial correlation (α=.05).

RESULTS

The polishing protocol exerted the highest influence on SR and SFE values (P<.001; SR: partial eta squared η=.970; SFE: η=.450), followed by material group (P<.001, SR: η=.319; SFE: η=.429). The interaction effect of the binary combinations of the 2 independent parameters (polishing protocol and material group) was also significant (P<.001, SR: η=.681; SFE: η=.365).

CONCLUSIONS

Chairside methods presented lower SR values than laboratory methods, and specimens polished using the 2-body mode showed higher SR than did specimens polished using the 3-body mode.

摘要

问题陈述

聚醚醚酮(PEEK)可作为固定义齿的基托材料。然而,关于实验室和椅旁抛光方法的信息仍然匮乏。

目的

本体外研究的目的是确定实验室和椅旁抛光方法对PEEK、自凝聚甲基丙烯酸甲酯及饰面复合树脂的表面粗糙度(SR)和表面自由能(SFE)的影响。

材料与方法

对3种材料中的每种材料制备80个样本(N = 240),并分为7个抛光组和1个对照组(n = 10)。7个组又分为4种实验室方案:抛光膏(Abraso)、第二种抛光膏(Opal L)、硅胶抛光器(Ceragum)和金刚石磨头(Diagen - Turbo磨头)。另外3个组为椅旁方案:彩虹技术(Super - Snap套件)、抛光膏(Prisma gloss)和抛光系统(Enhance finishing)。用SiC P4000进行机械抛光作为对照处理。测量各方案的平均SR和SFE,并通过扫描电子显微镜(SEM)评估其表面形貌。对经对数转换的数据采用协方差分析、双向和单向方差分析以及偏相关分析(α = 0.05)。

结果

抛光方案对SR和SFE值的影响最大(P < 0.001;SR:偏η² = 0.970;SFE:η = 0.450),其次是材料组(P < 0.001,SR:η = 0.319;SFE:η = 0.429)。两个独立参数(抛光方案和材料组)的二元组合的交互作用也很显著(P < 0.001,SR:η = 0.681;SFE:η = 0.365)。

结论

椅旁方法的SR值低于实验室方法,采用二体模式抛光的样本的SR高于采用三体模式抛光的样本。

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