Naji Ghassan Abdul-Hamid, Omar Ros Anita, Yahya Rosiyah
Department of Restorative Dentistry, Faculty of Dentistry, University of Malaya, Kuala Lumpur 50603, Malaysia; Department of Prosthetic Dentistry, College of Dentistry, University of Baghdad, Bab-Almoadham, P.O. Box 1417, Baghdad, Iraq.
Department of Restorative Dentistry, Faculty of Dentistry, University of Malaya, Kuala Lumpur 50603, Malaysia.
J Mech Behav Biomed Mater. 2017 Mar;67:135-143. doi: 10.1016/j.jmbbm.2016.12.007. Epub 2016 Dec 15.
In all-ceramic systems, a high incidence of veneer chip-off has been reported in clinical studies. Coefficient of thermal expansion (CTE) behaviour is one of the factors that may increase residual stress in the interface and influence the veneer/core bond strength. Therefore, this study aimed to evaluate the effect of sodalite zeolite-infiltration on the CTE behaviour and bond strength of different all-ceramic prostheses. The case-study groups were synthesized sodalite zeolite-infiltrated alumina (IA-SOD) and synthesized sodalite zeolite-infiltrated zirconia-toughened alumina (ZTA) (IZ-SOD), while the control groups were glass-infiltrated alumina (IA-glass) and glass-infiltrated ZTA (IZ-glass). Forty cylindrical-shaped samples measuring 5 mm in diameter and 10 mm in height were tested for CTE using a thermo-mechanical analyser machine, and forty disc-shaped ceramic samples measuring 12 mm in diameter and 1.2 ± 0.2 mm in thickness were prepared using specially designed stainless steel split mould and veneered by cylinder-shaped (2 mm high × 2 mm diameter) low-fusing porcelain (Vita VM7). The veneer/core samples were sintered and tested for shear bond strength using a high precision universal testing machine. Scanning electron microscope, stereo microscope, atomic force microscope, and energy-dispersive X-ray spectroscopy were used to investigate the structural characteristics of samples at the fracture surface. The collected data were analyzed with a one-way ANOVA and Tukey HSD test (α=.05). IZ-SOD revealed highest CTE and shear bond strength values, while the IA-glass revealed the lowest values than the other groups. There was no significant difference in CTE and bond strength among IZ-SOD, IA-SOD and IZ-glass samples (p>0.05). The experimental SOD zeolite-infiltrated samples revealed higher CTE mismatch and bond strength along with a more favourable mode of failure than did the commercial glass-infiltrated samples. Sandblast technique is considered as effective conditioning procedure for enhancing the surface roughness of SOD zeolite-infiltrated frameworks which subsequently improving the bond strength.
在全陶瓷系统中,临床研究报告了较高的贴面崩瓷发生率。热膨胀系数(CTE)行为是可能增加界面残余应力并影响贴面/核粘结强度的因素之一。因此,本研究旨在评估方钠石沸石渗透对不同全陶瓷修复体的CTE行为和粘结强度的影响。案例研究组为合成方钠石沸石渗透氧化铝(IA-SOD)和合成方钠石沸石渗透氧化锆增韧氧化铝(ZTA)(IZ-SOD),而对照组为玻璃渗透氧化铝(IA-玻璃)和玻璃渗透ZTA(IZ-玻璃)。使用热机械分析仪对40个直径5毫米、高10毫米的圆柱形样品进行CTE测试,并使用专门设计的不锈钢分体模具制备40个直径12毫米、厚度1.2±0.2毫米的盘形陶瓷样品,并用圆柱形(高2毫米×直径2毫米)低熔瓷(Vita VM7)进行贴面。将贴面/核样品烧结,并用高精度万能试验机测试其剪切粘结强度。使用扫描电子显微镜、立体显微镜、原子力显微镜和能量色散X射线光谱仪研究断裂表面样品的结构特征。收集的数据采用单因素方差分析和Tukey HSD检验(α = 0.05)进行分析。IZ-SOD显示出最高的CTE和剪切粘结强度值,而IA-玻璃显示出比其他组最低的值。IZ-SOD、IA-SOD和IZ-玻璃样品之间的CTE和粘结强度没有显著差异(p>0.05)。与商业玻璃渗透样品相比,实验性方钠石沸石渗透样品显示出更高的CTE不匹配和粘结强度,以及更有利的失效模式。喷砂技术被认为是一种有效的预处理程序,可提高方钠石沸石渗透框架的表面粗糙度,从而提高粘结强度。