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纳米技术在自酸蚀粘结系统中对不锈钢正畸托槽剪切粘结强度的影响。

Effect of nanotechnology in self-etch bonding systems on the shear bond strength of stainless steel orthodontic brackets.

作者信息

Hammad Shaza M, El-Wassefy Noha, Maher Ahmed, Fawakerji Shafik M

机构信息

University School of Dentistry, Mansoura, Egypt.

School of Dentistry, Mansoura University, Mansoura, Egypt.

出版信息

Dental Press J Orthod. 2017 Feb;22(1):47-56. doi: 10.1590/2177-6709.22.1.047-056.oar.

Abstract

OBJECTIVE

To evaluate the effect of silica dioxide (SiO2) nanofillers in different bonding systems on shear bond strength (SBS) and mode of failure of orthodontic brackets at two experimental times.

METHODS

Ninety-six intact premolars were divided into four groups: A) Conventional acid-etch and primer Transbond XT; B) Transbond Plus self-etch primer; and two self-etch bonding systems reinforced with silica dioxide nanofiller at different concentrations: C) Futurabond DC at 1%; D) Optibond All-in-One at 7%. Each group was allocated into two subgroups (n = 12) according to experimental time (12 and 24 hours). SBS test was performed using a universal testing machine. ARI scores were determined under a stereomicroscope. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were used to determine the size and distribution of nanofillers. One-way ANOVA was used to compare SBS followed by the post-hoc Tukey test. The chi-square test was used to evaluate ARI scores.

RESULTS

Mean SBS of Futurabond DC and Optibond All-in-One were significantly lower than conventional system, and there were no significant differences between means SBS obtained with all self-etch bonding systems used in the study. Lower ARI scores were found for Futurabond DC and Optibond All-in-One. There was no significant difference of SBS and ARI obtained at either time points for all bonding systems. Relative homogeneous distribution of the fillers was observed with the bonding systems.

CONCLUSION

Two nanofilled systems revealed the lowest bond strengths, but still clinically acceptable and less adhesive was left on enamel. It is advisable not to load the brackets immediately to the maximum.

摘要

目的

评估不同粘结系统中二氧化硅(SiO₂)纳米填料在两个实验时间点对正畸托槽剪切粘结强度(SBS)及破坏模式的影响。

方法

96颗完整的前磨牙被分为四组:A)传统酸蚀和底漆Transbond XT;B)Transbond Plus自酸蚀底漆;以及两种不同浓度二氧化硅纳米填料增强的自酸蚀粘结系统:C)1%的Futurabond DC;D)7%的Optibond All-in-One。根据实验时间(12小时和24小时),每组再分为两个亚组(n = 12)。使用万能试验机进行SBS测试。在体视显微镜下确定ARI评分。采用扫描电子显微镜(SEM)和透射电子显微镜(TEM)确定纳米填料的尺寸和分布。采用单因素方差分析比较SBS,随后进行事后Tukey检验。采用卡方检验评估ARI评分。

结果

Futurabond DC和Optibond All-in-One的平均SBS显著低于传统系统,本研究中使用的所有自酸蚀粘结系统获得的平均SBS之间无显著差异。Futurabond DC和Optibond All-in-One的ARI评分较低。所有粘结系统在任一时刻获得的SBS和ARI均无显著差异。观察到粘结系统中填料的相对均匀分布。

结论

两种纳米填料系统显示出最低的粘结强度,但仍在临床可接受范围内,且牙釉质上残留的粘结剂较少。建议不要立即将托槽加载到最大负荷。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7634/5398842/c80c763e2439/2176-9451-dpjo-22-01-00047-gf1.jpg

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