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载体对喷雾干燥风味物及其功能特性的影响。

Effects of Carriers on Spray-dried Flavors and Their Functional Characteristics.

作者信息

Farouk Amr, El-Kalyoubi Mamdouh, Ali Hatem, Mageed Magda Abd El, Khallaf Mohamed, Moawad Shimaa

出版信息

Pak J Biol Sci. 2020 Jan;23(3):257-263. doi: 10.3923/pjbs.2020.257.263.

Abstract

BACKGROUND AND OBJECTIVE

Encapsulation is an effective method to keep the quality of and avoid changes in flavors or essential oils due to oxidation, heating, volatilization, or chemical interactions. This study aims to microencapsulate key flavorings by traditional wall materials, namely, gum arabic (GA), maltodextrin (MD) and sodium caseinate (SC) and evaluate the effects of different wall materials on the properties of the flavor microcapsules.

MATERIALS AND METHODS

The emulsions of flavor compounds (linalool, citral, orange oil, allyl caproate and isoamyl acetate) were prepared using GA, SC and MD as carriers with different concentrations and then encapsulated in powder form by a spray dryer. Physical properties, including encapsulation efficiency, viscosity, emulsion stability and moisture, were studied before and after the spray drying process. Moreover, the morphology and extent of the nonenzymatic browning (NEB) of powder particles were performed using a scanning electron microscope (SEM) and a chroma meter. The effect of encapsulation on flavor retention and chemical composition was evaluated using gas chromatography-mass spectrometry (GC-MS).

RESULTS

Orange oil shows the maximum retention efficiency (84.5-97.9%), whereas isoamyl acetate is less retained during drying (44.4-72.5%) compared with other volatile compounds. Increasing the concentration of GA provides the highest retention for all aroma compounds and improves the viscosity and the emulsion stability of spray-dried powder. The presence of MD as the main encapsulating agent enables the formation of several homogeneous capsules with a good spherical shape and a smooth surface, according to SEM. The NEB is observed intensively in encapsulated samples containing citral and orange oils, whereas the least browning occurs in isoamyl acetate microcapsules.

CONCLUSION

Wall material formulation affects the retention, morphology and physical properties of the encapsulated flavors, which can be used in food or nutraceutical powder premixes.

摘要

背景与目的

微胶囊化是一种有效的方法,可保持风味物质或精油的品质,避免其因氧化、加热、挥发或化学相互作用而发生变化。本研究旨在用传统壁材(即阿拉伯胶(GA)、麦芽糊精(MD)和酪蛋白酸钠(SC))对关键调味剂进行微胶囊化,并评估不同壁材对风味微胶囊性能的影响。

材料与方法

以GA、SC和MD为载体,制备不同浓度的风味化合物(芳樟醇、柠檬醛、橙油、己酸烯丙酯和乙酸异戊酯)乳液,然后通过喷雾干燥将其制成粉末形式。在喷雾干燥前后研究了包括包封率、粘度、乳液稳定性和水分在内的物理性质。此外,使用扫描电子显微镜(SEM)和色度计对粉末颗粒的形态和非酶褐变(NEB)程度进行了研究。使用气相色谱-质谱联用仪(GC-MS)评估微胶囊化对风味保留和化学成分的影响。

结果

与其他挥发性化合物相比,橙油的保留效率最高(84.5 - 97.9%),而乙酸异戊酯在干燥过程中的保留率较低(44.4 - 72.5%)。增加GA的浓度可使所有香气化合物的保留率最高,并提高喷雾干燥粉末的粘度和乳液稳定性。根据SEM观察,以MD作为主要包封剂时可形成几个形状良好、表面光滑的均匀胶囊。在含有柠檬醛和橙油的微胶囊化样品中观察到强烈的NEB,而乙酸异戊酯微胶囊中的褐变最少。

结论

壁材配方会影响微胶囊化风味物质的保留、形态和物理性质,这些风味物质可用于食品或营养保健品粉末预混物中。

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