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尝试使用电子背散射衍射来验证ZnYO的存在。

Attempting to Verify the Existence of ZnYO Using Electron Backscatter Diffraction.

作者信息

Wisniewski Wolfgang, Švančárek Peter, Allix Mathieu

机构信息

CEMHTI UPR3079 CNRS, Univ. Orléans, Orléans F-45071, France.

Le Studium, Loire Valley Institute for Advanced Studies, Orléans & Tours 45000, France.

出版信息

ACS Omega. 2020 Jul 9;5(28):17576-17581. doi: 10.1021/acsomega.0c02043. eCollection 2020 Jul 21.

Abstract

Attempts to synthesize ZnYO are made via a solid-state reaction in a high-temperature X-ray powder diffraction chamber as well as analyzing YO sinter ceramics pressure infiltrated by ZnO in a scanning electron microscope using energy-dispersive X-ray spectroscopy and electron backscatter diffraction (EBSD). The microstructure of the sinter ceramic is composed of ZnO grains dispersed in an YO matrix. Superimposed EBSD patterns of YO are misindexed as ZnYO during the EBSD scan. The literature concerning ZnYO is critically discussed.

摘要

通过在高温X射线粉末衍射室中进行固态反应来尝试合成ZnYO,同时在扫描电子显微镜中使用能量色散X射线光谱和电子背散射衍射(EBSD)分析由ZnO压力渗透的YO烧结陶瓷。烧结陶瓷的微观结构由分散在YO基体中的ZnO晶粒组成。在EBSD扫描过程中,YO的叠加EBSD图案被误索引为ZnYO。对有关ZnYO的文献进行了批判性讨论。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c5cc/7377228/8849a18f4eda/ao0c02043_0001.jpg

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