Kim Hoe-Sung, Kim Jihyun, Choi Jisu, Paik Yujin, Moon Bokyung, Joo Yong-Sung, Lee Kwang-Won
Department of Biotechnology, College of Life Science and Biotechnology, Korea University, 145 Anam-ro, Seongbuk-gu, Seoul, 02841 Republic of Korea.
Department of Statistics, College of Natural Science, Dongguk University, Seoul, 04620 Republic of Korea.
Food Sci Biotechnol. 2021 Jul 6;30(7):989-1002. doi: 10.1007/s10068-021-00927-7. eCollection 2021 Jul.
Polycyclic aromatic hydrocarbons (PAHs) were analyzed using gas chromatography-mass spectrometry in 115 dairy products and beverages, including alcoholic, grain, carbonated, and functional drinks; fruit and vegetable juices; coffee; and tea, purchased from 10 local city markets in South Korea. The sample groups were divided into non-fatty and fatty groups, pretreated with the ultrasound-assisted extraction method and saponification method, respectively. The limit of detection, limit of quantification, and accuracy were 0.038-0.185 μg/kg, 0.114-0.560 μg/kg, and 87.64-112.25%, respectively. The measurement uncertainty was ≤ 6.38% for eight PAHs (PAH8). PAH8 was detected in 41 of the 115 samples, ranging from 0.041 to 7.793 µg/kg. The risk assessment revealed that the margin of exposure for PAH8 ranged from 3.60 × 10 to 7.84 × 10 in the mean intake groups and from 3.60 × 10 to 5.33 × 10 in the P97.5 intake groups.
The online version contains supplementary material available at 10.1007/s10068-021-00927-7.
采用气相色谱 - 质谱联用仪对从韩国10个当地城市市场购买的115种乳制品和饮料进行了多环芳烃(PAHs)分析。这些饮料包括酒精饮料、谷物饮料、碳酸饮料和功能性饮料;果蔬汁;咖啡;以及茶。样本组分为非脂肪组和脂肪组,分别采用超声辅助萃取法和皂化法进行预处理。检测限、定量限和准确度分别为0.038 - 0.185μg/kg、0.114 - 0.560μg/kg和87.64 - 112.25%。8种多环芳烃(PAH8)的测量不确定度≤6.38%。在115个样本中的41个样本中检测到了PAH8,含量范围为0.041至7.793µg/kg。风险评估显示,PAH8在平均摄入量组中的暴露边际范围为3.60×10至7.84×10,在P97.5摄入量组中的暴露边际范围为3.60×10至5.33×10。
在线版本包含可在10.1007/s10068 - 021 - 00927 - 7获取的补充材料。