Lu Yifan, Zhang Bo, Shen Huishan, Ge Xiangzhen, Sun Xiangxiang, Zhang Qian, Zhang Xiuyun, Sun Zhuangzhuang, Li Wenhao
College of Food Science and Engineering, Northwest A&F University, Xianyang 712100, China.
Foods. 2021 Dec 28;11(1):65. doi: 10.3390/foods11010065.
Lutein is a kind of vital carotenoid with high safety and significant advantages in biological functions. However, poor water solubility and stability of lutein have limited its application. This study selected different weight ratios of sodium caseinate to acetylated mung bean starch (10:0, 9:1, 7:3, 5:5, 3:7, 1:9, and 0:10) to prepare lutein emulsions, and the microcapsules were produced by spray drying technology. The microstructure, physicochemical properties, and storage stability of microcapsules were investigated. The results show that the emulsion systems were typical non-Newtonian fluids. Lutein microcapsules were light yellow fine powder with smooth and relatively complete particle surface. The increase of sodium caseinate content led to the enhanced emulsion effect of the emulsion and the yield and solubility of microcapsules increased, and wettability and the average particle size became smaller. The encapsulation efficiency of lutein microcapsules ranged from 69.72% to 89.44%. The thermal characteristics analysis showed that the endothermic transition of lutein microcapsules occurred at about 125 °C. The microcapsules with sodium caseinate as single wall material had the worst stability. Thus, it provides a reference for expanding the application of lutein in food, biological, pharmaceutical, and other industries and improving the stability and water dispersion of other lipid-soluble active ingredients.
叶黄素是一种重要的类胡萝卜素,具有高安全性且在生物学功能方面具有显著优势。然而,叶黄素较差的水溶性和稳定性限制了其应用。本研究选择不同重量比的酪蛋白酸钠与乙酰化绿豆淀粉(10:0、9:1、7:3、5:5、3:7、1:9和0:10)来制备叶黄素乳液,并通过喷雾干燥技术制备微胶囊。对微胶囊的微观结构、理化性质和储存稳定性进行了研究。结果表明,乳液体系为典型的非牛顿流体。叶黄素微胶囊为浅黄色细粉,颗粒表面光滑且相对完整。酪蛋白酸钠含量的增加导致乳液的乳化效果增强,微胶囊的产率和溶解度增加,润湿性提高且平均粒径变小。叶黄素微胶囊的包封率在69.72%至89.44%之间。热特性分析表明,叶黄素微胶囊的吸热转变发生在约125℃。以酪蛋白酸钠为单一壁材的微胶囊稳定性最差。因此,该研究为扩大叶黄素在食品、生物、制药等行业的应用以及提高其他脂溶性活性成分的稳定性和水分散性提供了参考。