Gigax Jonathan G, Chancey Matthew R, Xie Dongyue, Kim Hyosim, Wang Yongqiang, Maloy Stuart A, Li Nan
Operational Readiness and Implementation, Los Alamos National Lab, Los Alamos, NM 87545, USA.
Center for Integrated Nanotechnologies, Los Alamos National Lab, Los Alamos, NM 87545, USA.
Materials (Basel). 2022 Jun 15;15(12):4253. doi: 10.3390/ma15124253.
Small disks are often the specimen of choice for exposure in nuclear reactor environments, and this geometry invariably limits the types of mechanical testing that can be performed on the specimen. Recently, shear punch testing has been utilized to evaluate changes arising from neutron irradiation in test reactor environments on these small disk specimens. As part of a broader effort to link accelerated testing using ion irradiation and conventional neutron irradiation techniques, a novel microshear specimen geometry was developed for use with heavy-ion irradiated specimens. The technique was demonstrated in pure Cu irradiated to 11 and 110 peak dpa with 10 MeV Cu ions. At 11 peak dpa, the Cu specimen had a high density of small voids in the irradiated region, while at 110 peak dpa, larger voids with an average void swelling of ~20% were observed. Micropillar and microshear specimens both exhibited hardening at 11 dpa, followed by softening at 110 dpa. The close alignment of the new microshear technique and more conventional micropillar testing, and the fact that both follow intuition, is a good first step towards applying microshear testing to a wider range of irradiated materials.
小圆盘通常是核反应堆环境中暴露试验的首选试样,这种几何形状总是限制了对试样所能进行的机械测试类型。最近,剪切冲压试验已被用于评估试验反应堆环境中中子辐照对这些小圆盘试样产生的变化。作为将离子辐照加速试验与传统中子辐照技术联系起来的更广泛努力的一部分,开发了一种新型微剪切试样几何形状,用于重离子辐照试样。该技术在经10 MeV铜离子辐照至11和110峰值每原子位移损伤(dpa)的纯铜中得到了验证。在11峰值dpa时,铜试样在辐照区域有高密度的小空洞,而在110峰值dpa时,观察到平均空洞肿胀约20%的较大空洞。微柱和微剪切试样在11 dpa时均表现出硬化,随后在110 dpa时软化。新的微剪切技术与更传统的微柱测试的紧密一致性,以及两者都符合直觉这一事实,是将微剪切测试应用于更广泛辐照材料的良好第一步。