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不同环境条件下硅酸锂陶瓷的断裂

Fracture of Lithia Disilicate Ceramics under Different Environmental Conditions.

作者信息

Esquivel-Upshaw Josephine F, Hsu Shu-Min, Ren Fan, Stephany Jenna, Xia Xinyi, Chiu Chan-Wen, Neal Dan, Mecholsky John J

机构信息

Division of Prosthodontics, College of Dentistry, Restorative Dental Sciences, University of Florida, Gainesville, FL 32610, USA.

Department of Chemical Engineering, Herbert Wertheim College of Engineering, University of Florida, Gainesville, FL 32610, USA.

出版信息

Materials (Basel). 2022 Jul 29;15(15):5261. doi: 10.3390/ma15155261.

Abstract

The objective of this research was to quantify the effect of surface degradation and abrasion separately and in combination on the flexural strength of lithia disilicate ceramics. Lithia disilicate disks were fabricated using the lost wax technique and pressing in vacuum. The eight groups in this pilot experiment were (i) reference, hydrated in distilled water for 24 h prior to fracture; (ii) reference, non-hydrated group; (iii) 28-day pH cycling group; (iv) 125K chewing cycle group; (v) combined pH cycling + 125K chewing cycle; (vi) constant pH 2 solution for 28 days; (vii) constant pH 7 solution for 28 days; and (viii) constant pH 10 solution for 28 days. pH cycling is a method that alternates between pH 2, 7 and 10 over 28 days. A total of 15 disks were used for each group. All the groups were tested using the biaxial piston and a three-ball flexural strength test to obtain their biaxial flexural strength. pH 2 constant immersion demonstrated the highest fracture strength and was significantly greater than all other groups (p < 0.0001). Chewing and pH cycling + chewing groups exhibited the lowest fracture strengths and were significantly lower than all other groups (p < 0.0001). The damage observed from the chewing simulator does not represent apparent clinical fractures.

摘要

本研究的目的是分别量化表面降解和磨损及其组合对二硅酸锂陶瓷弯曲强度的影响。采用失蜡法并在真空中压制制备二硅酸锂圆盘。本初步实验中的八组分别为:(i)对照组,在断裂前于蒸馏水中水化24小时;(ii)对照组,非水化组;(iii)28天pH循环组;(iv)125K咀嚼循环组;(v)pH循环+125K咀嚼循环组合组;(vi)在pH 2的溶液中持续浸泡28天;(vii)在pH 7的溶液中持续浸泡28天;(viii)在pH 10的溶液中持续浸泡28天。pH循环是一种在28天内使pH值在2、7和10之间交替变化的方法。每组共使用15个圆盘。所有组均采用双轴活塞和三球弯曲强度试验进行测试,以获得其双轴弯曲强度。pH 2持续浸泡组显示出最高的断裂强度,且显著高于所有其他组(p < 0.0001)。咀嚼组以及pH循环+咀嚼组表现出最低的断裂强度,且显著低于所有其他组(p < 0.0001)。咀嚼模拟器观察到的损伤并不代表明显的临床骨折。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/eb52/9370032/2313f9d2c44f/materials-15-05261-g001.jpg

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