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七岛苔草纤维密度随直径变化的评估及热分析

Evaluation of the Change in Density with the Diameter and Thermal Analysis of the Seven-Islands-Sedge Fiber.

作者信息

Neuba Lucas de Mendonça, Junio Raí Felipe Pereira, Souza Andressa Teixeira, Ribeiro Matheus Pereira, da Silveira Pedro Henrique Poubel Mendonça, da Silva Thuane Teixeira, Pereira Artur Camposo, Monteiro Sergio Neves

机构信息

Department of Materials Science, Military Institute of Engineering-IME, Praça General Tíburcio, 80, Urca 222290-270, RJ, Brazil.

出版信息

Polymers (Basel). 2022 Sep 5;14(17):3687. doi: 10.3390/polym14173687.

Abstract

Basic properties of sedge fibers from the seven-islands-sedge plant () were investigated with possible application in reinforcing composite materials. A dimensional distribution and the effect of fiber diameter on density were investigated using gas pycnometry. The Weibull method, used to statistically analyze the acquired data from the diameter intervals, indicated an inverse dependence, where the thinnest fibers had the highest density values. The morphology of the fibers was obtained through scanning electron microscopy (SEM), in which a lower presence of defects was revealed in the thinner fibers, corroborating the inverse density dependence. In addition, the sedge fiber was characterized by differential scanning calorimetry and thermogravimetric analysis, which indicate an initial thermal degradation at around 241 °C. These results revealed for the first time that thinner sedge fibers might be promising reinforcement for polymer composites with a limit in temperature application.

摘要

研究了七岛苔草植物的莎草纤维的基本特性,探讨其在增强复合材料中的潜在应用。使用气体比重瓶法研究了尺寸分布以及纤维直径对密度的影响。采用威布尔方法对从直径区间获取的数据进行统计分析,结果表明存在反比关系,即最细的纤维密度值最高。通过扫描电子显微镜(SEM)观察纤维形态,发现较细的纤维中缺陷较少,这证实了密度的反比关系。此外,通过差示扫描量热法和热重分析对莎草纤维进行了表征,结果表明其初始热降解温度约为241℃。这些结果首次表明,较细的莎草纤维可能是温度应用受限的聚合物复合材料的有前景的增强材料。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/db70/9460121/0f40dfd09d22/polymers-14-03687-g001.jpg

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