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具有良好交互性和无线连接功能的便携式多通道电化学装置,用于现场检测。

Portable Multi-Channel Electrochemical Device with Good Interaction and Wireless Connection for On-Site Testing.

作者信息

Xu Yifei, Ning Haohao, Yu Shixin, Liu Shikun, Zhang Yan, Niu Chunyan, Zhang Yongzhuo, Low Sze Shin, Liu Jingjing

机构信息

School of Automation Engineering, Northeast Electric Power University, Jilin 132012, China.

Center for Advanced Measurement Science, National Institute of Metrology, Beijing 100029, China.

出版信息

Micromachines (Basel). 2023 Jan 5;14(1):142. doi: 10.3390/mi14010142.

Abstract

It is very important to rapidly test the key indicators of water in the field to fully evaluate the quality of the regional water environment. However, a high-resolution measuring device that can generate small currents for low-concentration analytes in water samples is often bulky, complex to operate, and difficult for data sharing. This work introduces a portable multi-channel electrochemical device with a small volume, good interaction, and data-sharing capabilities called PMCED. The PMCED provides an easy-to-operate graphical interactive interface to conveniently set the parameters for cyclic voltammetry or a differential pulse method performed by the four electrode channels. At the same time, the device, with a current sensitivity of 100 nA V, was applied to the detection of water samples with high background current and achieved a high-resolution measurement at low current levels. The PMCED uses the Narrow Band Internet of Things (NB-IoT) to meet the needs for uploading data to the cloud in remote areas. The electrochemical signal preprocessing and chemometrics models run in the cloud, and the final results are visualized on a web page, providing a remote access channel for on-site testing results.

摘要

快速检测现场水中的关键指标对于全面评估区域水环境质量非常重要。然而,一种能够为水样中的低浓度分析物产生小电流的高分辨率测量设备通常体积庞大、操作复杂且数据共享困难。这项工作介绍了一种名为PMCED的便携式多通道电化学设备,它体积小、交互性好且具备数据共享能力。PMCED提供了一个易于操作的图形交互界面,方便设置四个电极通道进行循环伏安法或差分脉冲法的参数。同时,该设备电流灵敏度为100 nA V,应用于高背景电流水样的检测,并在低电流水平下实现了高分辨率测量。PMCED利用窄带物联网(NB-IoT)来满足偏远地区将数据上传到云端的需求。电化学信号预处理和化学计量学模型在云端运行,最终结果在网页上可视化,为现场测试结果提供了远程访问渠道。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/dd8b/9866627/a08967fed506/micromachines-14-00142-g001.jpg

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