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原子力显微镜单晶硅探针尖端磨损的实验研究。

Experimental Investigation of Tip Wear of AFM Monocrystalline Silicon Probes.

机构信息

School of Mechanical Engineering, Tianjin University, Tianjin 300350, China.

School of Engineering, University of Warwick, Coventry CV4 7AL, UK.

出版信息

Sensors (Basel). 2023 Apr 18;23(8):4084. doi: 10.3390/s23084084.

Abstract

AFM has a wide range of applications in nanostructure scanning imaging and fabrication. The wear of AFM probes has a significant impact on the accuracy of nanostructure measurement and fabrication, which is particularly significant in the process of nanomachining. Therefore, this paper focuses on the study of the wear state of monocrystalline silicon probes during nanomachination, in order to achieve rapid detection and accurate control of the probe wear state. In this paper, the wear tip radius, the wear volume, and the probe wear rate are used as the evaluation indexes of the probe wear state. The tip radius of the worn probe is detected by the nanoindentation Hertz model characterization method. The influence of single machining parameters, such as scratching distance, normal load, scratching speed, and initial tip radius, on probe wear is explored using the single factor experiment method, and the probe wear process is clearly divided according to the probe wear degree and the machining quality of the groove. Through response surface analysis, the comprehensive effect of various machining parameters on probe wear is determined, and the theoretical models of the probe wear state are established.

摘要

原子力显微镜(AFM)在纳米结构扫描成像和制造方面具有广泛的应用。AFM 探针的磨损对纳米结构测量和制造的准确性有重大影响,在纳米加工过程中尤为重要。因此,本文专注于研究单晶硅探针在纳米加工过程中的磨损状态,以实现探针磨损状态的快速检测和精确控制。在本文中,将磨损探针的尖端半径、磨损体积和探针磨损率用作探针磨损状态的评估指标。使用纳米压痕赫兹模型特征化方法检测磨损探针的尖端半径。采用单因素实验方法探索了单个加工参数(如划痕距离、法向载荷、划痕速度和初始尖端半径)对探针磨损的影响,并根据探针磨损程度和槽加工质量清晰地划分了探针磨损过程。通过响应面分析,确定了各种加工参数对探针磨损的综合影响,并建立了探针磨损状态的理论模型。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d397/10141055/98e65b5b7fe3/sensors-23-04084-g001.jpg

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