Santos Jhenifer Cristina Carvalho, Correa Jefferson Luiz Gomes, Furtado Maria Luiza Bianchetti, de Morais Larissa Carolina, Borges Soraia Vilela, de Oliveira Cassiano Rodrigues, de Resende Jaime Vilela, de Oliveira Letícia Fernandes
Department of Food Science, Universidade Federal de Lavras, Lavras, MG, Brasil.
Department of Food Science, Universidade Federal de Lavras, Lavras, MG, Brasil.
Ultrason Sonochem. 2024 May;105:106868. doi: 10.1016/j.ultsonch.2024.106868. Epub 2024 Apr 3.
The use of extracts rich in bioactive compounds is becoming increasingly common in the food, cosmetics, and pharmaceutical industries for the production of functional products. Araticum is a potential fruit to be analyzed due to its content of phenolic compounds, carotenoids and vitamins, with antioxidant properties. Therefore, this study aimed to investigate the effect of ultrasound on total phenolic compounds, total carotenoids, ascorbic acid, color, turbidity and rheology in araticum juice. Response surface methodology based on a central composite design was applied. Araticum juice was subjected to sonication at amplitude levels ranging from 20 to 100 % of the total power (400 W) at a constant frequency of 20 kHz for different durations (2 to 10 min). Morphological analysis was conducted to observe microscopic particles, and viscosity and suitability to rheological models (Newtonian, Power Law, and Herschel-Bulkley) were assessed. The ultrasonic probe extraction method was compared to the control juice. According to the responses, using the desirability function, the optimal conditions for extraction were determined to be low power (low amplitude) applied in a short period of time or low power applied in a prolonged time. These conditions allowed an ultrasonic probe to act on releasing bioactive compounds without degrading them. All three rheological models were suitable, with the Power Law model being the most appropriate, exhibiting non-Newtonian pseudoplastic behavior.
富含生物活性化合物的提取物在食品、化妆品和制药行业用于生产功能性产品的应用越来越普遍。由于其含有具有抗氧化特性的酚类化合物、类胡萝卜素和维生素,刺果番荔枝是一种有待分析的潜在水果。因此,本研究旨在探究超声处理对刺果番荔枝汁中总酚类化合物、总类胡萝卜素、抗坏血酸、颜色、浊度和流变学的影响。采用基于中心复合设计的响应面法。将刺果番荔枝汁在20kHz的恒定频率下,以总功率(400W)的20%至100%的振幅水平进行不同时长(2至10分钟)的超声处理。进行形态分析以观察微观颗粒,并评估其粘度和对流变学模型(牛顿模型、幂律模型和赫谢尔-布尔克利模型)的适用性。将超声探头提取法与对照汁进行比较。根据响应结果,使用期望函数确定最佳提取条件为在短时间内施加低功率(低振幅)或在长时间内施加低功率。这些条件可使超声探头在不降解生物活性化合物的情况下作用于释放它们。所有三种流变学模型均适用,其中幂律模型最为合适,表现出非牛顿假塑性行为。