College of Materials Science and Engineering, Central South University of Forestry and Technology, Changsha 410004, Hunan, China.
College of Materials Science and Engineering, Central South University of Forestry and Technology, Changsha 410004, Hunan, China; Institute of Natural Products Research and Development, Central South University of Forestry and Technology, Changsha 410004, Hunan, China.
Int J Biol Macromol. 2024 Oct;277(Pt 4):134215. doi: 10.1016/j.ijbiomac.2024.134215. Epub 2024 Jul 27.
The utilization and economic benefits of biomass resources can be maximized through rational design and process optimization. In this study, an innovative approach for the simultaneous extraction of essential oil and lignin from Cinnamomum camphora leaves by deep eutectic solvent (DES) and optimization of the process parameters was achieved using deep learning tools. With the water content of 40 %, liquid-solid ratio of 9.00 mL/g, and distillation time of 51.81 min, the yields of the essential oil and lignin reached 3.15 ± 0.02 % and 9.75 ± 0.15 %, respectively. Notably, the efficiency of simultaneous extraction of essential oil improved by 23 % compared to that of traditional steam distillation. Moreover, the extraction mechanism of the process was clarified. The connection between lignin with cellulose and hemicellulose was disintegrated by the DES, resulting in lignin shedding and hence accelerating the dissolution of essential oil. Moreover, the compositions of lignin and essential oil were also identified.
通过合理的设计和过程优化,可以最大限度地利用生物质资源的利用和经济效益。在这项研究中,通过深度学习工具,实现了用深共晶溶剂(DES)从樟树叶中同时提取精油和木质素的创新方法,并对工艺参数进行了优化。在水含量为 40%、液固比为 9.00 mL/g 和蒸馏时间为 51.81 min 的条件下,精油和木质素的产率分别达到 3.15±0.02%和 9.75±0.15%。值得注意的是,与传统的水蒸气蒸馏相比,同时提取精油的效率提高了 23%。此外,还阐明了该过程的提取机制。DES 破坏了木质素与纤维素和半纤维素的连接,导致木质素脱落,从而加速了精油的溶解。此外,还鉴定了木质素和精油的成分。