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5摩尔%和3摩尔%氧化钇稳定氧化锆组合的牙科氧化锆的快速烧结对其透明度、乳光和微观结构的影响

Impact of Speed Sintering on Translucency, Opalescence and Microstructure of Dental Zirconia with a Combination of 5 mol% and 3 mol% Yttria-Stabilized Zirconia.

作者信息

Cho Mi-Hyang, Seol Hyo-Joung

机构信息

Department of Dental Laboratory, Wonkwang Health Science University, Iksan-si 54538, Republic of Korea.

Department of Dental Materials, Dental and Life Science Institute, School of Dentistry, Pusan National University, Yangsan-si 50612, Republic of Korea.

出版信息

Materials (Basel). 2024 Oct 22;17(21):5148. doi: 10.3390/ma17215148.

Abstract

Optical characteristics and microstructure of multilayered zirconia with different yttria contents in each layer can be influenced differently with a layer after speed sintering. The layer-wise translucency and opalescence of dental zirconia (E.max, E.max ZirCAD prime; Cercon, Cercon ht ML) after conventional (control) and speed sintering were analyzed using a spectrophotometer (n = 5). Specimens were subjected to microstructural analyses (n = 2) using field-emission scanning electron microscopy (FE-SEM) and phase analyses (n = 1) using high-resolution X-ray diffraction (HRXRD) and Rietveld refinement. The translucency parameter (TP) and opalescence parameter (OP) were analyzed using a 3-way ANOVA, followed by Scheffé's post hoc test (α = 0.05). The average grain size was analyzed using the Welch's -test and Kruskal-Wallis test, followed by the Bonferroni-Dunn post hoc test (α = 0.05). Changes to the TP and OP after speed sintering were only observed in the dentin layers. Although the TP of E.max increased ( < 0.05), the difference was below the 50:50% perceptibility threshold (ΔE = 0.8). The OP of E.max decreased slightly, whereas that of Cercon increased slightly ( < 0.05). The microstructure and phase fraction of both zirconia barely changed. Therefore, speed sintering is considered to have a negligible clinical impact on the optical characteristics and microstructure.

摘要

在快速烧结后,每层中具有不同氧化钇含量的多层氧化锆的光学特性和微观结构可能会受到不同的影响。使用分光光度计(n = 5)分析了传统(对照)烧结和快速烧结后牙科氧化锆(E.max、E.max ZirCAD prime;Cercon、Cercon ht ML)的逐层半透明度和乳光。使用场发射扫描电子显微镜(FE-SEM)对样本进行微观结构分析(n = 2),并使用高分辨率X射线衍射(HRXRD)和Rietveld精修进行相分析(n = 1)。使用三因素方差分析,随后进行Scheffé事后检验(α = 0.05)来分析半透明度参数(TP)和乳光参数(OP)。使用Welch's检验和Kruskal-Wallis检验,随后进行Bonferroni-Dunn事后检验(α = 0.05)来分析平均晶粒尺寸。仅在牙本质层中观察到快速烧结后TP和OP的变化。尽管E.max的TP增加了(P < 0.05),但差异低于50:50%的可感知阈值(ΔE = 0.8)。E.max的OP略有下降,而Cercon的OP略有增加(P < 0.05)。两种氧化锆的微观结构和相分数几乎没有变化。因此,快速烧结被认为对光学特性和微观结构的临床影响可忽略不计。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/47d8/11547037/162b6b915619/materials-17-05148-g001.jpg

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