Advances in Resistant Starch Research from Agro-Industrial Waste: A Bibliometric Analysis of Scientific Trends.

This study comprehensively analysed the scientific production of the extraction, characterisation, and toxicological risk of resistant starches obtained from agro-industrial by-products. Articles indexed in the Scopus database between 2015 and 2025 were analysed. The results showed a progressive increase in publications led by Chinese institutions, the most notable being Jiangnan University. Most of the studies were published in high-impact journals, with the International Journal of Biological Macromolecules standing out, followed by Carbohydrate Polymers and Food Chemistry, all in the first quartile. Most studies focused on extraction methods (physical, chemical, and mechanical) and starch characterisation (morphological, structural, molecular, physicochemical, and functional). Emerging trends are directed towards innovative applications such as functional foods. However, the risks associated with contaminants in reusing agro-industrial by-products have not been adequately explored, showing an important gap in the current scientific literature. In this context, future research should focus on evaluating toxicological risks derived from these processes, considering the presence and behaviour of heavy metals, pesticides, and mycotoxins, as well as the possible migration of chemical compounds generated during extraction.