Büyükpolat Murat, Çal İrem Kübra, Eryılmaz Bilge, Ersöz Bilge, Aydın Numan, Karaoğlanoğlu Serpil
Gulhane Faculty of Dentistry, Department of Restorative Dental Treatment, University of Health Sciences, Ankara, Turkey.
BMC Oral Health. 2025 Sep 3;25(1):1401. doi: 10.1186/s12903-025-06813-6.
The aim of this study was to investigate the effect of post-polymerization time and curing device type on the surface roughness, microhardness and color change of 3D printed permanent resin materials.
In this study, permanent resin samples with a layer print thickness of 50 μm and dimensions of 10 × 2 mm3 were produced on SLA and DLP printers. The samples were post-polymerized in blue LED and UV LED curing devices for 10, 20, 40 and 60 min. Initial surface roughness, microhardness and color values of all polymerized samples were measured. The samples were then aged (5000 cycles) and surface roughness, microhardness and color values were measured again. Data were evaluated using two-way analysis of variance (ANOVA) and Tukey post hoc test (p < 0.05).
There was no statistically significant difference in surface roughness when the samples produced in SLA and DLP printer were polymerized using blue LED and UV LED curing device for different durations (p > 0.05). The samples produced in SLA printer showed higher microhardness value when polymerized with UV LED for longer time (p < 0.05). There was no statistically significant difference in the microhardness values of DLP samples when polymerized with blue LED and UV LED (p > 0.05). When the samples produced in SLA and DLP printer were polymerized using blue LED and UV LED curing device for different durations, the color change and whiteness index increased as the post-polymerization time increased (p < 0.05). The surface roughness of the samples after aging did not change statistically significantly, while the microhardness value decreased (p < 0.05).
The post-polymerization time and the type of polymerization device do not affect the surface roughness of the 3D printed samples, but increase the microhardness value. Post-polymerization time increases the color change and whiteness index values of the samples. Post-polymerization of 3D printer permanent resin materials has an effect on the mechanical and optical properties of the material.
The post polymerization time of 3D resin materials and the type of curing device change the microhardness, color change and surface roughness of the material. This may affect the clinical success of the restoration.
本研究旨在探讨后聚合时间和固化设备类型对3D打印永久性树脂材料的表面粗糙度、显微硬度和颜色变化的影响。
在本研究中,在SLA和DLP打印机上制作层打印厚度为50μm、尺寸为10×2mm³的永久性树脂样品。样品在蓝色LED和UV LED固化设备中后聚合10、20、40和60分钟。测量所有聚合样品的初始表面粗糙度、显微硬度和颜色值。然后使样品老化(5000次循环),并再次测量表面粗糙度、显微硬度和颜色值。使用双向方差分析(ANOVA)和Tukey事后检验(p<0.05)对数据进行评估。
当使用蓝色LED和UV LED固化设备在不同时间对SLA和DLP打印机生产的样品进行聚合时,表面粗糙度没有统计学上的显著差异(p>0.05)。当SLA打印机生产的样品用UV LED长时间聚合时,显示出更高的显微硬度值(p<0.05)。当DLP样品用蓝色LED和UV LED聚合时,显微硬度值没有统计学上的显著差异(p>0.05)。当使用蓝色LED和UV LED固化设备在不同时间对SLA和DLP打印机生产的样品进行聚合时,颜色变化和白度指数随着后聚合时间的增加而增加(p<0.05)。老化后样品的表面粗糙度没有统计学上的显著变化,而显微硬度值下降(p<0.05)。
后聚合时间和聚合设备类型不影响3D打印样品的表面粗糙度,但会增加显微硬度值。后聚合时间会增加样品的颜色变化和白度指数值。3D打印机永久性树脂材料的后聚合对材料的机械和光学性能有影响。
3D树脂材料的后聚合时间和固化设备类型会改变材料的显微硬度、颜色变化和表面粗糙度。这可能会影响修复体的临床成功率。