Shimamine M, Takahashi K, Nakahara Y
Eisei Shikenjo Hokoku. 1993(111):66-74.
The reference standards of N-Ethyl methylenedioxyamphetamine, N-Hydroxy methylenedioxy-amphetamine, Mecloqualone, 4-Methylaminorex. Phendimetrazine and Phenmetrazine were chemically prepared from commercial chemicals. Their purities determined by HPLC were more than 99.8%. The standard spectra and chromatograms of the standards such as TLC, UV, IR, HPLC, GC/MS and NMR were measured. For the identification of these six drugs in forensic laboratory, their mass fragmentation and NMR spectra were discussed.
N-乙基亚甲二氧基苯丙胺、N-羟基亚甲二氧基苯丙胺、甲氯喹酮、4-甲基氨基苯丙胺、苯双甲吗啉和苯甲吗啉的参考标准品由市售化学品化学合成制备。通过高效液相色谱法测定,其纯度均超过99.8%。测定了这些标准品的薄层色谱、紫外光谱、红外光谱、高效液相色谱、气相色谱/质谱和核磁共振谱等标准光谱和色谱图。为了在法医实验室鉴定这六种药物,对它们的质谱裂解和核磁共振谱进行了讨论。