Johnson A, Shareef M Y, Walsh J M, Hatton P V, van Noort R, Hill R G
Department of Restorative Dentistry, University of Sheffield, UK.
Dent Mater. 1998 Nov;14(6):412-6. doi: 10.1016/s0300-5712(99)00015-9.
To assess the effect of mould and glass casting temperatures on the biaxial flexural strength (BFS) of two different types of castable glass-ceramic, using existing laboratory equipment and techniques.
Two castable glass-ceramic materials were evaluated. One glass (LG3) is based on SiO2-Al2O3-P2O5-CaO-CaF2, and is similar in composition to glasses used in the manufacture of glass-ionomer cements. The other glass (SG3) is based on SiO2-K2O-Na2O-CaO-CaF2, and is a canasite-based material. Both materials were used to produce discs of 12 mm diameter and 2 mm thickness using the same lost-wax casting process as used for metal castings. Mould temperatures of between 500 degrees C and 1000 degrees C and glass casting temperatures of between 1100 degrees C and 1450 degrees C were evaluated. The cast discs were cerammed and the biaxial flexural strength determined with a Lloyd 2000 R tester.
A significant difference was found for the BFS in the range of mould temperatures evaluated, with the optimum investment mould temperature being 590 degrees C for LG3 and 610 degrees C for SG3 (p = 0.0002 and p = 0.019, respectively). No significant differences were seen between any of the glass casting temperatures evaluated.
The mould temperature for castable glass-ceramic materials produced using the lost-wax casting process can have a significant effect on BFS. The optimum mould temperature may differ slightly depending on the type of material being used. The glass casting temperature of these materials does not appear to have a significant effect on BFS.
使用现有的实验室设备和技术,评估铸模温度和玻璃浇铸温度对两种不同类型可铸玻璃陶瓷双轴弯曲强度(BFS)的影响。
对两种可铸玻璃陶瓷材料进行评估。一种玻璃(LG3)基于SiO₂ - Al₂O₃ - P₂O₅ - CaO - CaF₂,其成分与用于制造玻璃离子水门汀的玻璃相似。另一种玻璃(SG3)基于SiO₂ - K₂O - Na₂O - CaO - CaF₂,是一种以硅钛钠钾矿为基础的材料。两种材料都采用与金属铸造相同的失蜡铸造工艺制作直径12毫米、厚度2毫米的圆盘。评估了500℃至1000℃的铸模温度以及1100℃至1450℃的玻璃浇铸温度。将铸好的圆盘进行陶瓷化处理,并用Lloyd 2000 R测试仪测定双轴弯曲强度。
在所评估的铸模温度范围内,双轴弯曲强度存在显著差异,LG3的最佳包埋铸模温度为590℃,SG3为610℃(分别为p = 0.0002和p = 0.019)。在所评估的任何玻璃浇铸温度之间均未观察到显著差异。
采用失蜡铸造工艺生产的可铸玻璃陶瓷材料的铸模温度会对双轴弯曲强度产生显著影响。最佳铸模温度可能会因所用材料类型而略有不同。这些材料的玻璃浇铸温度似乎对双轴弯曲强度没有显著影响。