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可压制修复陶瓷的力学性能评估

Mechanical property evaluation of pressable restorative ceramics.

作者信息

Drummond J L, King T J, Bapna M S, Koperski R D

机构信息

Department of Restorative Dentistry, College of Dentistry, University of Illinois at Chicago, 801 S. Paulina Street, Chicago, IL 60612-7212, USA.

出版信息

Dent Mater. 2000 May;16(3):226-33. doi: 10.1016/s0109-5641(00)00013-0.

Abstract

OBJECTIVE

The aim of this study was to evaluate the flexure strength under static and cyclic loading and the fracture toughness under static loading of six restorative ceramic materials. Specifically the intent was to compare four leucite (K2O.Al2O(3).4SiO2) strengthened feldspathic (pressable) porcelains (OA, OI, E, and FP) to a low fusing feldspathic porcelain (F) and an experimental (EC) lithium disilicate containing ceramic.

METHODS

All materials were tested as a control in air and distilled water (without aging) and after three months aging in air or distilled water to determine flexure strength and fracture toughness. A staircase approach was used to determine the cyclic flexure strength. EDS and SEM analysis were conducted on the polished and fracture surfaces.

RESULTS

The mean flexure strength for the controls in air and water (without aging or cyclic loading) ranged from 67 to 99 MPa, except the experimental ceramic that was twice as strong with a mean flexure strength of 191-205 MPa. For the mean fracture toughness, the range was 1.1-1.9 MPa/m0.5 with the experimental ceramic being 2.7 MPa/m0.5. The effect of testing in water and aging for three months caused a moderate reduction in the mean flexure strength (6-17%), and a moderate to severe reduction in the mean fracture toughness (5-39%). The largest decrease (15-60%) in mean flexure strength was observed when the samples were subjected to cyclic loading.

SIGNIFICANCE

The lithium disilicate containing ceramic had a significantly higher flexure strength and fracture toughness when compared to the four pressable leucite strengthened ceramics and the low fusing conventional porcelain. All of the leucite containing pressable ceramics did provide an increase in mean flexure strength (17-19%) and mean fracture toughness (3-64%) over the conventional feldspathic porcelain. Further, the influence of testing environment and loading conditions implies that these ceramic materials in the oral cavity might be susceptible to cyclic fatigue, resulting in a significant decrease in the survival time of all-ceramic restorations.

摘要

目的

本研究旨在评估六种修复陶瓷材料在静态和循环加载下的弯曲强度以及静态加载下的断裂韧性。具体而言,目的是将四种白榴石(K2O.Al2O(3).4SiO2)增强的长石质(可压铸)瓷(OA、OI、E和FP)与一种低熔点长石质瓷(F)和一种含二硅酸锂的实验性陶瓷(EC)进行比较。

方法

所有材料在空气中和蒸馏水中(未老化)作为对照进行测试,并在空气中或蒸馏水中老化三个月后测定弯曲强度和断裂韧性。采用阶梯法测定循环弯曲强度。对抛光表面和断裂表面进行能谱分析(EDS)和扫描电子显微镜(SEM)分析。

结果

在空气中和水中(未老化或循环加载)的对照样品的平均弯曲强度范围为67至99兆帕,除了实验性陶瓷的强度是其两倍,平均弯曲强度为191 - 205兆帕。对于平均断裂韧性,范围为1.1 - 1.9兆帕/米0.5,而实验性陶瓷为2.7兆帕/米0.5。在水中测试和老化三个月的影响导致平均弯曲强度适度降低(6 - 17%),平均断裂韧性中度至重度降低(5 - 39%)。当样品承受循环加载时,观察到平均弯曲强度最大降幅(15 - 60%)。

意义

与四种可压铸的白榴石增强陶瓷和低熔点传统瓷相比,含二硅酸锂的陶瓷具有显著更高的弯曲强度和断裂韧性。所有含白榴石的可压铸陶瓷相比传统长石质瓷,平均弯曲强度确实提高了(17 - 19%),平均断裂韧性提高了(3 - 64%)。此外,测试环境和加载条件的影响表明,口腔中的这些陶瓷材料可能易受循环疲劳影响,导致全瓷修复体的存活时间显著缩短。

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