Peutzfeldt A, Asmussen E
Department of Dental Materials, School of Dentistry, University of Copenhagen, Denmark.
J Dent. 2000 Aug;28(6):447-52. doi: 10.1016/s0300-5712(00)00021-x.
To determine the effect of different postcuring methods on degree of conversion, mechanical properties, and in vitro wear of two resin composites (Z100 and Charisma). The postcuring methods involved devices for inlay curing as well as devices present for other purposes in many dental laboratories or dental offices.
Specimens of the resin composites were initially light cured and then postcured according to one of the following methods: Translux EC handheld curing unit (10min), Translux EC light box (10min), Triad II (10min), 40 degrees C (10min), 70 or 110 degrees C for 10min, 1, 6, or 24h. The properties were determined following storage of the specimens for 1week in water at 37 degrees C. The degree of conversion was determined using transmission IR. The mechanical properties tested were diametral tensile strength, flexural strength, and flexural modulus. In vitro wear was induced by a three-body wear simulator.
Most postcuring methods increased degree of conversion of both materials. Postcuring increased the mechanical properties and in vitro wear resistance of Charisma, whereas no effect of postcuring was found on these properties of Z100.
Postcuring with the use of devices readily available in the dental laboratory and dental office increased the degree of conversion of Z100 and Charisma as well as the mechanical properties and in vitro wear resistance of Charisma. A heat treatment at 110 degrees C for 10-60min was found to be the most promising postcuring method.
确定不同后固化方法对两种树脂复合材料(Z100和卡瑞斯玛)的转化率、力学性能及体外磨损的影响。后固化方法涉及嵌体固化设备以及许多牙科实验室或牙科诊所中用于其他目的的设备。
树脂复合材料试件先进行光固化,然后根据以下方法之一进行后固化:Translux EC手持式固化单元(10分钟)、Translux EC灯箱(10分钟)、Triad II(10分钟)、40℃(10分钟)、70或110℃10分钟、1、6或24小时。在37℃水中储存1周后测定性能。使用透射红外光谱法测定转化率。测试的力学性能包括径向拉伸强度、弯曲强度和弯曲模量。体外磨损由三体磨损模拟器诱导。
大多数后固化方法提高了两种材料的转化率。后固化提高了卡瑞斯玛的力学性能和体外耐磨性,而对Z100的这些性能未发现后固化的影响。
使用牙科实验室和牙科诊所中容易获得的设备进行后固化,提高了Z100和卡瑞斯玛的转化率以及卡瑞斯玛的力学性能和体外耐磨性。发现110℃热处理10 - 60分钟是最有前景的后固化方法。