Park Joung-Man, Lee Sang-Il, Kim Ki-Won, Yoon Dong-Jin
Department of Polymer Science & Engineering, Research Center for Aircraft Parts Technology, Gyeongsang National University, Chinju, 660-701, Korea
J Colloid Interface Sci. 2001 May 1;237(1):80-90. doi: 10.1006/jcis.2001.7426.
Interfacial adhesion and nondestructive behavior of the electrodeposited (ED) carbon fiber reinforced composites were evaluated using the electro-micromechanical technique and acoustic emission (AE). Interfacial shear strength (IFSS) of the ED carbon fiber/epoxy composites was higher than that of the untreated case. This might be expected because of the possible chemical and hydrogen bonding based on an electrically adsorbed polymeric interlayer. Logarithmic electrical resistivity of the untreated single-carbon fiber composite increased suddenly to infinity when the fiber fracture occurred, whereas that of the ED composite increased relatively broadly up to infinity. This may be due to the retarded fracture time as a result of the enhanced IFSS. In single- and 10-carbon fiber composites, the number of AE signals coming from the interlayer failure of the ED carbon fiber composite was much larger than that of the untreated composite. As the number of each first fiber fracture increased in the 10-carbon fiber composite, the electrical resistivity increased stepwise, and the slope of logarithmic electrical resistance increased. In the three-graphite filament composite with a narrow 1 time inter-filament distance, the total numbers of the filament fracture and the IFSS were smaller than those of the wider 5 times case. This might be because the interacting fracture energy caused by a filament break could affect the adjacent filaments. Copyright 2001 Academic Press.
采用电微机械技术和声发射(AE)对电沉积(ED)碳纤维增强复合材料的界面粘附和无损行为进行了评估。ED碳纤维/环氧树脂复合材料的界面剪切强度(IFSS)高于未处理的情况。由于基于电吸附聚合物中间层可能存在的化学键合和氢键作用,这可能是预期的结果。当纤维断裂发生时,未处理的单碳纤维复合材料的对数电阻率突然增加到无穷大,而ED复合材料的对数电阻率则相对较宽地增加到无穷大。这可能是由于IFSS增强导致断裂时间延迟。在单根和10根碳纤维复合材料中,来自ED碳纤维复合材料中间层失效的AE信号数量远多于未处理的复合材料。随着10根碳纤维复合材料中每根第一根纤维断裂数量的增加,电阻率逐步增加,对数电阻的斜率增大。在细丝间距为1倍的窄间距三石墨细丝复合材料中细丝断裂总数和IFSS小于细丝间距为5倍的宽间距情况。这可能是因为细丝断裂引起的相互作用断裂能会影响相邻细丝。版权所有2001年学术出版社。