Ellakwa A, Shortall A, Shehata M, Marquis P
The University of Birmingham, The School of Dentistry, St Chad's Queensway, England.
Oper Dent. 2001 Sep-Oct;26(5):467-75.
This study investigated the influence of fiber reinforcement on the flexural properties of four commercial (Artglass, Belleglass HP, Herculite XRV and Solidex) veneering composites (Series A) and two experimental composites (Series B&C). This study investigated how the composition of the veneering composites influenced the enhancement of strength and modulus produced by fiber reinforcement. The formulation of the experimental composites were varied by changing the filler load (Series B) or the resin matrix chemistry (Series C) to assess the effect these changes would have on the degree of reinforcement. In Series A, the commercial veneering composites were reinforced by an Ultra-High-Molecular-Weight Polyethylene fiber (UHMW-PE/Connect) to evaluate flexural properties after 24 hours and six months. In Series B, experimental composites with the same organic matrix but with different filler loads (40% to 80% by weight) were also reinforced by Connect fiber to evaluate flexural properties. In Series C, experimental composites (Systems 1-4) with the same filler load (76.5% by weight) but with different organic matrix compositions were reinforced by Connect fiber to evaluate flexural properties. For Series B and C, flexural properties were evaluated after 24 hours water storage. All the samples were prepared in a mold 2 mm x 2 mm x 25 mm and stored in distilled water at 37 degrees C until they were ready for flexural testing in an Instron Universal Testing Machine using a crosshead speed of 1 mm/minute. The results showed no significant differences in the flexural strength (FS) between any of the commercial reinforced composites in Series A. The flexural modulus (FM) of the fiber-reinforced Belleglass HP group was significantly higher than for Artglass and Solidex. Water storage for six months had no significant (p>0.05) effect on the flexural strength of three of the four reinforced veneering composites. The flexural strength for Artglass was significantly reduced (p<0.05) by six-month water storage. In Series B, however, increasing the amount of filler loading improved the flexural modulus of the reinforced experimental composite but had no effect on its flexural strength. In Series C, changing the organic matrix formulation had no affect on flexural strength but affected the flexural modulus of the reinforced experimental composite.
本研究调查了纤维增强对四种商用(Artglass、Belleglass HP、Herculite XRV和Solidex)饰面复合材料(A系列)以及两种实验性复合材料(B系列和C系列)弯曲性能的影响。本研究还调查了饰面复合材料的成分如何影响纤维增强所带来的强度和模量的提高。通过改变填料含量(B系列)或树脂基体化学组成(C系列)来改变实验性复合材料的配方,以评估这些变化对增强程度的影响。在A系列中,商用饰面复合材料用超高分子量聚乙烯纤维(UHMW-PE/Connect)进行增强,以评估24小时和六个月后的弯曲性能。在B系列中,具有相同有机基体但填料含量不同(重量百分比为40%至80%)的实验性复合材料也用Connect纤维进行增强,以评估弯曲性能。在C系列中,具有相同填料含量(重量百分比为76.5%)但有机基体组成不同的实验性复合材料(系统1-4)用Connect纤维进行增强,以评估弯曲性能。对于B系列和C系列,在储存24小时后评估弯曲性能。所有样品均在2毫米×2毫米×25毫米的模具中制备,并储存在37摄氏度的蒸馏水中,直至准备好在Instron万能材料试验机上以1毫米/分钟的十字头速度进行弯曲测试。结果表明,A系列中任何商用增强复合材料之间的弯曲强度(FS)均无显著差异。纤维增强的Belleglass HP组的弯曲模量(FM)显著高于Artglass和Solidex。六个月的水储存对四种增强饰面复合材料中的三种的弯曲强度没有显著(p>0.05)影响。六个月的水储存使Artglass的弯曲强度显著降低(p<0.05)。然而,在B系列中,增加填料含量提高了增强实验性复合材料的弯曲模量,但对其弯曲强度没有影响。在C系列中,改变有机基体配方对弯曲强度没有影响,但影响了增强实验性复合材料的弯曲模量。