Guo D H, Xia L
Shanghai Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China, Shanghai 200135, China.
Se Pu. 2001 May;19(3):276-8.
A method for the quantitative determination of 11 organic acids (oxalic acid, citric acid, tartaric acid, malic acid, ascorbic acid, lactic acid, succinic acid, formic acid, acetic acid, glutaric acid and fumaric acid) in fruit juice was developed successfully. It was based on an ion exclusion chromatographic separation under the conditions of isocratic elution with 17 mmol/L sulphuric acid solution with the ICE-ION-300 ion exclusion column, and the UV detection at 210 nm. The precision of the method was investigated and the relative standard deviations were from 1.5% to 9.8% (n = 10).
成功开发了一种定量测定果汁中11种有机酸(草酸、柠檬酸、酒石酸、苹果酸、抗坏血酸、乳酸、琥珀酸、甲酸、乙酸、戊二酸和富马酸)的方法。该方法基于在使用ICE-ION-300离子排斥柱、以17 mmol/L硫酸溶液等度洗脱的条件下进行离子排斥色谱分离,并在210 nm处进行紫外检测。研究了该方法的精密度,相对标准偏差为1.5%至9.8%(n = 10)。