Watanabe Ikuya, Liu Jie, Atsuta Mitsuru, Okabe Toru
Department of Biomaterials Science, Baylor College of Dentistry, Texas A&M University System Health Science Center, 3302 Gaston Ave., Dallas, TX 75246, USA.
Am J Dent. 2003 Aug;16(4):231-4.
To examine the effect of welding method and heat treatment on the strength of laser-welded gold alloy with age-hardenability at intraoral temperature.
Cast gold alloy plates (0.5 x 3.0 x 20 mm3) were prepared and cut perpendicular to the 3.0 mm surface of the plate. After the cut halves were fixed in a jig, they were laser-welded using a Nd: YAG laser. Three laser pulses were applied from one side (single-welded) or both sides (double-welded) to weld the entire joint width of the specimens. Three different heat treatments were given the specimens: solution treatment at 700 degrees C for 5 minute (ST), aging at 250 degrees C for 15 minute after ST (HA), and aging at 37 degrees C for 3 day after ST (IA). As-cast specimens were also reserved. Uncut specimens served as non-welded control specimens. Tensile testing was conducted at a crosshead speed of 2 mm/minute and a gauge length of 10 mm. The breaking stress (Bs: MPa) was recorded, and the data (n = 5 per group) were statistically analyzed.
In the control groups, the Bs values of the IA were not significantly different (P > 0.05) from those of the HA specimens. The laser-welded IA specimens showed significantly greater (P < 0.05) Bs values compared to the solution-treated and as-cast specimens. The double-welded specimens showed significantly greater Bs values compared to the single-welded specimens after any heat treatment.
研究焊接方法和热处理对具有口腔温度时效硬化特性的激光焊接金合金强度的影响。
制备铸造金合金板(0.5×3.0×20mm³),并垂直于板的3.0mm表面切割。将切割后的两半固定在夹具中,使用Nd:YAG激光进行激光焊接。从一侧(单焊)或两侧(双焊)施加三个激光脉冲,以焊接试样的整个接头宽度。对试样进行三种不同的热处理:在700℃下固溶处理5分钟(ST),在ST后于250℃时效15分钟(HA),以及在ST后于37℃时效3天(IA)。还保留铸态试样。未切割的试样用作非焊接对照试样。以2mm/分钟的十字头速度和10mm的标距进行拉伸试验。记录断裂应力(Bs:MPa),并对数据(每组n = 5)进行统计分析。
在对照组中,IA的Bs值与HA试样的Bs值无显著差异(P>0.05)。与固溶处理和铸态试样相比,激光焊接的IA试样显示出显著更高(P<0.05)的Bs值。在任何热处理后,双焊试样的Bs值均显著高于单焊试样。