Zhang Yu-mei, Guo Tian-wen, Shen Li-juan, Li Zuo-chen
Prosthodontic Department, College of Stomatology, The Fourth Military Medical University, Xi'an 710032, China.
Hua Xi Kou Qiang Yi Xue Za Zhi. 2004 Dec;22(6):516-8.
To investigate the influence of mold temperature on the mechanical properties of Ti-Zr alloy castings.
Ti-Zr alloy was cast into a mold which was made of a zircon (ZrO2.SiO2) investment with a casting machine (China) designed as vacuum, pressure and centrifuge. At three mold temperatures (room temperature, 300 degrees C, 600 degrees C) the Ti-Zr alloy was cast separately. The ultimate tensile strength (sigmab), 0.2% offset yield point strength (sigma0.2), and elongation to fracture (delta) were determined by a universal testing machine with 15 mm pre-marked gauge interval. The surface micro-structures of Ti-Zr alloy castings at three mold temperatures were observed by optical microscope.
At a higher mold temperature during casting, the tensile strength and yield strength of Ti-Zr alloy were significantly increased, while the elongations were significantly decreased. The micro-structure of the surface was different from the inner part. There was a reacted layer in the outermost surface. The thickness of reacted layers at the three mold temperatures was about 35.5 man (room temperature), 55.0 microm (300 degrees C) and 65.5 microm (600 degrees C), respectively. The inner part of microstructure composed of main a phases within the prior alpha grain boundaries.
The mold temperature is one of the major factors influencing Ti-Zr alloy mechanical properties. Comparing with Ti6Al4V alloy and Co-Cr alloy castings, Ti-Zr alloy is more suitable for denture frame.
研究铸型温度对Ti-Zr合金铸件力学性能的影响。
采用真空、压力和离心铸造机(中国产),将Ti-Zr合金铸入由锆英砂(ZrO2.SiO2)包埋材料制成的铸型中。在三个铸型温度(室温、300℃、600℃)下分别铸造Ti-Zr合金。用标距为15mm的万能试验机测定其抗拉强度(σb)、0.2%屈服强度(σ0.2)和断裂伸长率(δ)。用光学显微镜观察三个铸型温度下Ti-Zr合金铸件的表面微观结构。
铸造时铸型温度较高时,Ti-Zr合金的抗拉强度和屈服强度显著提高,而伸长率显著降低。表面微观结构与内部不同。最外层有一个反应层。三个铸型温度下反应层的厚度分别约为35.5μm(室温)、55.0μm(300℃)和65.5μm(600℃)。微观结构内部由先共析α晶界内的主要α相组成。
铸型温度是影响Ti-Zr合金力学性能的主要因素之一。与Ti6Al4V合金和Co-Cr合金铸件相比,Ti-Zr合金更适合制作义齿支架。