Toellner T S, Alatas A, Said A, Shu D, Sturhahn W, Zhao J
Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439, USA.
J Synchrotron Radiat. 2006 Mar;13(Pt 2):211-5. doi: 10.1107/S0909049505042664. Epub 2006 Feb 17.
The design and performance results for a cryogenically stabilized high-resolution monochromator for 23.880 keV (lambda = 52 pm) X-rays are presented. The four-crystal-reflection monochromator is suitable for nuclear resonant scattering measurements from 119Sn compounds using synchrotron radiation. The design includes a low-vibration cryostat that maintains two of the four crystal reflections at a temperature where the coefficient for thermal expansion of the crystalline material (silicon) vanishes. Test results demonstrate a 1.3 meV bandwidth with negligible broadening due to vibrations and a spectral efficiency of 37% when used with an undulator source.
本文介绍了一款用于23.880 keV(波长=52皮米)X射线的低温稳定高分辨率单色仪的设计及性能结果。该四晶体反射单色仪适用于利用同步辐射对119Sn化合物进行核共振散射测量。其设计包括一个低振动低温恒温器,该恒温器可将四个晶体反射中的两个维持在晶体材料(硅)热膨胀系数为零的温度。测试结果表明,该单色仪带宽为1.3毫电子伏特,因振动产生的展宽可忽略不计,与波荡器源配合使用时光谱效率为37%。