Danesh Gholamreza, Lippold Carsten, Ziebura Thomas, Reinhardt Klaus-Jürgen, Schäfer Edgar, Ehmer Ulrike
Department of Orthodontics and Dentofacial Orthopedics, University of Münster, Münster, Germany.
J Orofac Orthop. 2006 Mar;67(2):127-37. doi: 10.1007/s00056-006-5031-6.
It was the aim of the present study to investigate the material properties of different resins and their suitability for the fabrication of occlusal and intermaxillary splints.
We subjected auto-polymerized resins (Palapress, Orthocryl, Steady-Resin M) and light-polymerized resins (Acrylight, Primosplint, Triad TranSheet Colorless and Pink) to investigation. The Targis Power light oven was used to polymerize the light-cured resins. After the auto-polymerized resins had been mixed by hand and filled into the forms, they were polymerized for 15 minutes in a high-pressure polymerization machine (Palamat) at 2 bar. The parameters examined were flexural strength, water adsorption, and polymerization shrinkage. Tests carried out according to DIN EN ISO 1567 served to determine flexural strength, flexural modulus, and water adsorption. Polymerization shrinkage was determined via the buoyancy test.
The resins' flexural strength ranged from 60 to 101 MPa. Flexural moduli lay between 1.3 and 5.3 GPa. The water adsorption noted in light-cured resins amounted to 2.1-4.6 mass percent. Palapress and Steady-Resin displayed the lowest water adsorption with 2.0 mass percent. The light-polymerized resins revealed significantly less shrinkage (p < 0.05) than the autopolymerized resins tested in this study.
Our results demonstrate that the light-cured resins-with the exception of Acrylight -easily match and even exceed the material properties of the cold-polymerized resins regarding flexural strength, flexural modulus, water adsorption and polymerization shrinkage. The light-cured resins examined thus seem suitable for use as splint material.
本研究旨在调查不同树脂的材料性能及其用于制作咬合夹板和颌间夹板的适用性。
我们对自凝树脂(Palapress、Orthocryl、Steady-Resin M)和光固化树脂(Acrylight、Primosplint、Triad TranSheet无色和粉色)进行了研究。使用Targis Power光固化机对光固化树脂进行聚合。自凝树脂手工混合并填入模具后,在高压聚合机(Palamat)中于2巴压力下聚合15分钟。所检测的参数包括弯曲强度、吸水性和聚合收缩率。根据DIN EN ISO 1567进行的测试用于测定弯曲强度、弯曲模量和吸水性。通过浮力测试确定聚合收缩率。
树脂的弯曲强度范围为60至101兆帕。弯曲模量在1.3至5.3吉帕之间。光固化树脂的吸水量为2.1 - 4.6质量百分比。Palapress和Steady-Resin的吸水量最低,为2.0质量百分比。本研究中测试的光固化树脂的收缩率明显低于自凝树脂(p < 0.05)。
我们的结果表明,除Acrylight外,光固化树脂在弯曲强度、弯曲模量、吸水性和聚合收缩率方面很容易达到甚至超过冷聚合树脂的材料性能。因此,所检测的光固化树脂似乎适合用作夹板材料。