超声辐照下制备水溶性富勒烯[C70]
Preparation of a water-soluble fullerene [C70] under ultrasonic irradiation.
作者信息
Ko Weon-Bae, Park Young-Hwan, Jeong Min-Kyu
机构信息
Department of Chemistry, Sahmyook University, 26-21 Kongneung 2-Dong, Nowon Ku, Seoul 139-742, Republic of Korea.
出版信息
Ultrasonics. 2006 Dec 22;44 Suppl 1:e367-9. doi: 10.1016/j.ultras.2006.05.004. Epub 2006 Jun 2.
PMID:16814829
Abstract
A water-soluble fullerene [C(70)] is prepared with fullerene [C(70)] and a mixture of concd. sulfuric acid (H(2)SO(4)) and concd. nitric acid (HNO(3)) at the ratio (v/v) of 3:1 under ultrasonic irradiation at 25-43 degrees C. The MALDI-TOF-MS spectra confirmed that the product of a water-soluble fullerene compound was C(70).
摘要
一种水溶性富勒烯[C(70)]是通过富勒烯[C(70)]与浓硫酸（H(2)SO(4)）和浓硝酸（HNO(3)）按3:1的体积比混合，并在25 - 43摄氏度的超声辐射下制备而成。基质辅助激光解吸电离飞行时间质谱（MALDI-TOF-MS）光谱证实该水溶性富勒烯化合物的产物为C(70)。
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