Liu Hai-tao, Zhang Ben-gang, Chen Jian-min, Xue Jian
Institute of Medicinal Plant Development, Chinese Academy of Medical Sciences, Peking Union Medical College, Beijing 100094, China.
Zhongguo Zhong Yao Za Zhi. 2006 Nov;31(22):1841-6.
The current methods to prepare and determine pesticide residues in Chinese herbal medicine were summarized in this paper. In addition,the new techniques to prepare and determine pesticide residues used in recent years was reviewed, which included solid-phase micro-extraction (SPME) , supercritical fluid extraction ( SFE) , accelerated solvent extraction (ASE) , immune affinity chromatography (IAC), supercritical fluid chromatography (SFC), column switching high performance liquid chromatography (CSHPLC), high performance liquid chromatography/mass spectrometry (HPLC/MS), capillary electrophoresis (CE) and capillary zone electrophoresis (CZE) , and immune analysis (IA), etc. To sum up, these would bring a great progress in analysis of the pesticide residues in Chinese herbal medicine, and make it more rapidly, accurately and normatively.
本文综述了目前中药材中农药残留的制备与测定方法。此外,还对近年来用于制备和测定农药残留的新技术进行了综述,包括固相微萃取(SPME)、超临界流体萃取(SFE)、加速溶剂萃取(ASE)、免疫亲和色谱(IAC)、超临界流体色谱(SFC)、柱切换高效液相色谱(CSHPLC)、高效液相色谱/质谱(HPLC/MS)、毛细管电泳(CE)和毛细管区带电泳(CZE)以及免疫分析(IA)等。综上所述,这些将给中药材中农药残留的分析带来巨大进步,并使其更加快速、准确和规范。